methyl 2,3,4-tri-O-benzyl-6-O-(4-(3,4-dimethoxyphenyl)benzyl)-α-D-glucopyranoside

Base Information

• Chemical Name: methyl 2,3,4-tri-O-benzyl-6-O-(4-(3,4-dimethoxyphenyl)benzyl)-α-D-glucopyranoside
• CAS No.: 760987-63-1
• Molecular Formula: C₄₃H₄₆O₈
• Molecular Weight: 690.833

Synonyms:methyl 2,3,4-tri-O-benzyl-6-O-(4-(3,4-dimethoxyphenyl)benzyl)-α-D-glucopyranoside

Chemical Property of methyl 2,3,4-tri-O-benzyl-6-O-(4-(3,4-dimethoxyphenyl)benzyl)-α-D-glucopyranoside

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Technology Process of methyl 2,3,4-tri-O-benzyl-6-O-(4-(3,4-dimethoxyphenyl)benzyl)-α-D-glucopyranoside

There total 1 articles about methyl 2,3,4-tri-O-benzyl-6-O-(4-(3,4-dimethoxyphenyl)benzyl)-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

3,4-Dimethoxyphenylboronic acid (122775-35-3) + (2R,3R,4S,5R,6S)-3,4,5-tris(benzyloxy)-2-(((4-bromobenzyl)oxy)methyl)-6-methoxytetrahydro-2H-pyran (760987-62-0) → methyl 2,3,4-tri-O-benzyl-6-O-(4-(3,4-dimethoxyphenyl)benzyl)-α-D-glucopyranoside (760987-63-1)

Guidance literature:

With potassium phosphate; tetrabutylammomium bromide; palladium diacetate; In ethanol; at 20 ℃;

DOI:10.1039/b407324j

Reference yield: 100.0%

5-methyl-1,3-benzodioxole (7145-99-5) + methyl 2,3,4-tri-O-benzyl-6-O-(4-(3,4-dimethoxyphenyl)benzyl)-α-D-glucopyranoside (760987-63-1) → methyl 2,3,4-tri-O-benzyl-D-glucopyranoside (53008-65-4,641635-63-4) + 6-(4-(3,4-dimethoxyphenyl)benzyl)-3,4-(methylenedioxy)toluene (1434832-13-9)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1021/jo4004184

Reference yield: 85.0%

methyl 2,3,4-tri-O-benzyl-6-O-(4-(3,4-dimethoxyphenyl)benzyl)-α-D-glucopyranoside (760987-63-1) → methyl 2,3,4-tri-O-benzyl-D-glucopyranoside (53008-65-4,641635-63-4)

Guidance literature:

With water; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 20 ℃; for 3h;

DOI:10.1039/b407324j

upstream raw materials:

3,4-Dimethoxyphenylboronic acid

(2R,3R,4S,5R,6S)-3,4,5-tris(benzyloxy)-2-(((4-bromobenzyl)oxy)methyl)-6-methoxytetrahydro-2H-pyran

Downstream raw materials:

methyl 2,3,4-tri-O-benzyl-D-glucopyranoside

(2R,3R,4S,5R,6S)-3,4,5-tris(benzyloxy)-2-(((4-bromobenzyl)oxy)methyl)-6-methoxytetrahydro-2H-pyran

6-(4-(3,4-dimethoxyphenyl)benzyl)-3,4-(methylenedioxy)toluene

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