ethyl 5-(3-azidophenyl)-1-(pyrrol-3-yl)-2-methylpyrrole-2',3-dicarboxylate

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Chemical Name:ethyl 5-(3-azidophenyl)-1-(pyrrol-3-yl)-2-methylpyrrole-2',3-dicarboxylate
CAS No.:410538-48-6
Molecular Formula:C₂₁H₂₁N₅O₄
Molecular Weight:407.429
Hs Code.:

Synonyms:ethyl 5-(3-azidophenyl)-1-(pyrrol-3-yl)-2-methylpyrrole-2',3-dicarboxylate

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Chemical Property of ethyl 5-(3-azidophenyl)-1-(pyrrol-3-yl)-2-methylpyrrole-2',3-dicarboxylate

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Technology Process of ethyl 5-(3-azidophenyl)-1-(pyrrol-3-yl)-2-methylpyrrole-2',3-dicarboxylate

There total 4 articles about ethyl 5-(3-azidophenyl)-1-(pyrrol-3-yl)-2-methylpyrrole-2',3-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 410538-45-3
ethyl 5-(3-aminophenyl)-1-(pyrrol-3-yl)-2-methylpyrrole-2',3-dicarboxylate

: 410538-48-6
ethyl 5-(3-azidophenyl)-1-(pyrrol-3-yl)-2-methylpyrrole-2',3-dicarboxylate

Guidance literature:: ethyl 5-(3-aminophenyl)-1-(pyrrol-3-yl)-2-methylpyrrole-2',3-dicarboxylate; With acetic acid; sodium nitrite; In water; at 0 - 5 ℃; for 1h;

With sodium azide; In water; acetic acid; at 20 ℃; for 24h;
DOI:10.1016/S0040-4020(01)01033-X

Reference yield:

: 118209-48-6
ethyl 1-(3-nitrophenyl)-1,4-pentanedione-3-carboxylate

: 410538-48-6
ethyl 5-(3-azidophenyl)-1-(pyrrol-3-yl)-2-methylpyrrole-2',3-dicarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 40 percent / AcOH / Heating

2.1: 90 percent / H₂ / Pd/C / ethanol / 20 °C / 2585.74 Torr

3.1: NaNO₂; acOH / H₂O / 1 h / 0 - 5 °C

3.2: 85 percent / NaN₃ / H₂O; acetic acid / 24 h / 20 °C

With hydrogen; acetic acid; sodium nitrite; palladium on activated charcoal; In ethanol; water;
DOI:10.1016/S0040-4020(01)01033-X

Reference yield:

: 252932-48-2
3-amino-2-ethoxycarbonylpyrrole

: 410538-48-6
ethyl 5-(3-azidophenyl)-1-(pyrrol-3-yl)-2-methylpyrrole-2',3-dicarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 40 percent / AcOH / Heating

2.1: 90 percent / H₂ / Pd/C / ethanol / 20 °C / 2585.74 Torr

3.1: NaNO₂; acOH / H₂O / 1 h / 0 - 5 °C

3.2: 85 percent / NaN₃ / H₂O; acetic acid / 24 h / 20 °C

With hydrogen; acetic acid; sodium nitrite; palladium on activated charcoal; In ethanol; water;
DOI:10.1016/S0040-4020(01)01033-X