(E)-4-(N-cyclohexyl-N-hydroxyamino)-2-butenyl azide

Base Information Edit

Chemical Name:(E)-4-(N-cyclohexyl-N-hydroxyamino)-2-butenyl azide
CAS No.:118149-84-1
Molecular Formula:C₁₀H₁₈N₄O
Molecular Weight:210.279
Hs Code.:
Mol file:118149-84-1.mol

Synonyms:(E)-4-(N-cyclohexyl-N-hydroxyamino)-2-butenyl azide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-4-(N-cyclohexyl-N-hydroxyamino)-2-butenyl azide Edit

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Technology Process of (E)-4-(N-cyclohexyl-N-hydroxyamino)-2-butenyl azide

There total 2 articles about (E)-4-(N-cyclohexyl-N-hydroxyamino)-2-butenyl azide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Acetic acid (E)-4-(cyclohexyl-hydroxy-amino)-but-2-enyl ester

: 118149-84-1
(E)-4-(N-cyclohexyl-N-hydroxyamino)-2-butenyl azide

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium azide; In tetrahydrofuran; water; Yield given; Ambient temperature;
DOI:10.1021/jo00275a011

Reference yield:

: 85669-62-1
(Z)-4-acetoxy-2-buten-1-yl diethyl phosphate

: 2211-64-5
N-cyclohexyl-hydroxylamine

: 118149-84-1
(E)-4-(N-cyclohexyl-N-hydroxyamino)-2-butenyl azide

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium azide; Yield given. Multistep reaction; 1) THF, room temp.; 2) THF, room temp.;
DOI:10.1016/0040-4039(88)85061-5