Ph(Me₃SiO)CNMo(N(tert-Bu)C₆H₃(CH₃)2)3

Base Information

• Chemical Name: Ph(Me₃SiO)CNMo(N(tert-Bu)C₆H₃(CH₃)2)3
• CAS No.: 916221-07-3
• Molecular Formula: C₄₆H₆₈MoN₄OSi
• Molecular Weight: 817.098

Synonyms:Ph(Me₃SiO)CNMo(N(tert-Bu)C₆H₃(CH₃)2)3

Chemical Property of Ph(Me₃SiO)CNMo(N(tert-Bu)C₆H₃(CH₃)2)3

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Ph(Me₃SiO)CNMo(N(tert-Bu)C₆H₃(CH₃)2)3

There total 1 articles about Ph(Me₃SiO)CNMo(N(tert-Bu)C₆H₃(CH₃)2)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

tetrahydrofuran (109-99-9,24979-97-3,77392-70-2) + [Mo(N((t)Bu)(C6H3-3,5-Me2))3NC(O)Ph]O3SCF3 (819799-81-0) + magnesium anthracene + trimethylsilyl trifluoromethanesulfonate (27607-77-8) → Ph(Me3SiO)CNMo(N(tert-Bu)C6H3(CH3)2)3 (916221-07-3)

Guidance literature:

In diethyl ether; treatment of molybdenum compd. with magnesium anthracene, treatment withtrimethylsilyl deriv. in ether;

DOI:10.1021/ja066090a

Reference yield: 93.0%

Ph(Me3SiO)CNMo(N(tert-Bu)C6H3(CH3)2)3 (916221-07-3) + tin(ll) chloride → Mo(IV)Cl(N(t-Bu)(3,5-C6H3Me2))3 (251306-52-2)

Guidance literature:

byproducts: PhCN; treatment of molybdenum compd. with tin compd. for 1 h; filtration;

DOI:10.1021/ja066090a

Reference yield: 20.0%

Ph(Me3SiO)CNMo(N(tert-Bu)C6H3(CH3)2)3 (916221-07-3) + zinc(II) chloride (7646-85-7,24359-56-6) → Mo(IV)Cl(N(t-Bu)(3,5-C6H3Me2))3 (251306-52-2)

Guidance literature:

byproducts: PhCN; treatment of molybdenum compd. with zinc compd. for 3 h; crystn.;

DOI:10.1021/ja066090a

upstream raw materials:

tetrahydrofuran

[Mo(N((t)Bu)(C₆H₃-3,5-Me₂))3NC(O)Ph]O₃SCF₃

trimethylsilyl trifluoromethanesulfonate

Downstream raw materials:

Mo(IV)Cl(N(t-Bu)(3,5-C₆H₃Me₂))3

NMo(N[((t)Bu)(3,5-C₆H₃Me₂)])3

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 916221-07-3 Ph(Me₃SiO)CNMo(N(tert-Bu)C₆H₃(CH₃)2)3

Send

Send

Metric Ton KG G Pound L ML

Send

Send