2-bromo-3-(3-chloro-4-fluorophenyl)-3,4-dihydro-2H-benzo[e][1,3,2]oxazaphosphinine

Base Information

Chemical Name:2-bromo-3-(3-chloro-4-fluorophenyl)-3,4-dihydro-2H-benzo[e][1,3,2]oxazaphosphinine
CAS No.:950694-17-4
Molecular Formula:C₁₃H₉BrClFNOP
Molecular Weight:360.55
Hs Code.:

Synonyms:2-bromo-3-(3-chloro-4-fluorophenyl)-3,4-dihydro-2H-benzo[e][1,3,2]oxazaphosphinine

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Chemical Property of 2-bromo-3-(3-chloro-4-fluorophenyl)-3,4-dihydro-2H-benzo[e][1,3,2]oxazaphosphinine

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Technology Process of 2-bromo-3-(3-chloro-4-fluorophenyl)-3,4-dihydro-2H-benzo[e][1,3,2]oxazaphosphinine

There total 1 articles about 2-bromo-3-(3-chloro-4-fluorophenyl)-3,4-dihydro-2H-benzo[e][1,3,2]oxazaphosphinine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 329779-41-1
α-(3-chloro-4-fluoroaniline)-2-cresol

: 950694-17-4
2-bromo-3-(3-chloro-4-fluorophenyl)-3,4-dihydro-2H-benzo[e][1,3,2]oxazaphosphinine

Guidance literature:: With phosphorus tribromide; triethylamine; In toluene; at 50 ℃; for 3h;
DOI:10.1021/jf070850z

Reference yield:

: 2420-26-0
4-chlorosalicylaldehyde

: 950694-17-4
2-bromo-3-(3-chloro-4-fluorophenyl)-3,4-dihydro-2H-benzo[e][1,3,2]oxazaphosphinine

: 950694-25-4
[3-(3-chloro-4-fluorophenyl)-2-oxo-3,4-dihydro-2H-2λ⁵-benzo[e][1,3,2]oxazaphosphinin-2-yl]-2-hydroxy-4-chlorophenylmethanol

Guidance literature:: 2-bromo-3-(3-chloro-4-fluorophenyl)-3,4-dihydro-2H-benzo[e][1,3,2]oxazaphosphinine; With water; triethylamine; In toluene; at 25 ℃; for 2h;

4-chlorosalicylaldehyde; With niobium(V) oxide; triethylamine; In toluene; at 50 ℃; for 2h; Further stages.;
DOI:10.1021/jf070850z

Reference yield:

: 950694-17-4
2-bromo-3-(3-chloro-4-fluorophenyl)-3,4-dihydro-2H-benzo[e][1,3,2]oxazaphosphinine

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 950694-23-2
[3-(3-chloro-4-fluorophenyl)-2-oxo-3,4-dihydro-2H-2λ⁵-benzo[e][1,3,2]oxazaphosphinin-2-yl]-4-hydroxyphenylmethanol

Guidance literature:: 2-bromo-3-(3-chloro-4-fluorophenyl)-3,4-dihydro-2H-benzo[e][1,3,2]oxazaphosphinine; With water; triethylamine; In toluene; at 25 ℃; for 2h;

4-hydroxy-benzaldehyde; With niobium(V) oxide; triethylamine; In toluene; at 50 ℃; for 1.3h; Further stages.;
DOI:10.1021/jf070850z