1-Methoxy-N-<4-(1,1-dimethylethyl)phenylmethyl>-N-methyl-4-indolmethanamin

Base Information

Chemical Name:1-Methoxy-N-<4-(1,1-dimethylethyl)phenylmethyl>-N-methyl-4-indolmethanamin
CAS No.:143425-24-5
Molecular Formula:C₂₂H₂₈N₂O
Molecular Weight:336.477
Hs Code.:

Synonyms:1-Methoxy-N-<4-(1,1-dimethylethyl)phenylmethyl>-N-methyl-4-indolmethanamin

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Chemical Property of 1-Methoxy-N-<4-(1,1-dimethylethyl)phenylmethyl>-N-methyl-4-indolmethanamin

Chemical Property:

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Technology Process of 1-Methoxy-N-<4-(1,1-dimethylethyl)phenylmethyl>-N-methyl-4-indolmethanamin

There total 5 articles about 1-Methoxy-N-<4-(1,1-dimethylethyl)phenylmethyl>-N-methyl-4-indolmethanamin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 143425-20-1
1-Methoxy-N-<4-(1,1-dimethylethyl)phenylmethyl>-N-methyl-4-indolcarboxamid

: 143425-24-5
1-Methoxy-N-<4-(1,1-dimethylethyl)phenylmethyl>-N-methyl-4-indolmethanamin

Guidance literature:: With sodium bis(2-methoxyethoxy)aluminium dihydride; In toluene; for 1h; Ambient temperature;
DOI:10.1002/ardp.19923250711

Reference yield:

: 1975-50-4
2-methyl-3-nitrobenzic acid

: 143425-24-5
1-Methoxy-N-<4-(1,1-dimethylethyl)phenylmethyl>-N-methyl-4-indolmethanamin

Guidance literature:: Multi-step reaction with 6 steps

1: SOCl₂ / 3 h / Heating

2: Et₃N / diethyl ether / 1 h / Ambient temperature

3: dimethylformamide / 7 h / 110 - 115 °C

4: H₂ / 10percent Pd/C / tetrahydrofuran / 41 h / Ambient temperature

5: 1.) NaH / 1.) DMF, r.t., 15 min, 2.) 15 min

6: 90 percent / RedAl^R / toluene / 1 h / Ambient temperature

With thionyl chloride; hydrogen; sodium hydride; triethylamine; sodium bis(2-methoxyethoxy)aluminium dihydride; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide; toluene;
DOI:10.1002/ardp.19923250711

Reference yield:

: 143425-13-2
N-(4-tert-Butyl-benzyl)-N-methyl-3-nitro-2-((E)-2-pyrrolidin-1-yl-vinyl)-benzamide

: 143425-24-5
1-Methoxy-N-<4-(1,1-dimethylethyl)phenylmethyl>-N-methyl-4-indolmethanamin

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / 10percent Pd/C / tetrahydrofuran / 41 h / Ambient temperature

2: 1.) NaH / 1.) DMF, r.t., 15 min, 2.) 15 min

3: 90 percent / RedAl^R / toluene / 1 h / Ambient temperature

With hydrogen; sodium hydride; sodium bis(2-methoxyethoxy)aluminium dihydride; palladium on activated charcoal; In tetrahydrofuran; toluene;
DOI:10.1002/ardp.19923250711