butyl 4-(4-methoxy-2-methyl-3,6-dioxo-5-tridecylcyclohexa-1,4-dienylamino)butanoate

Base Information

Chemical Name:butyl 4-(4-methoxy-2-methyl-3,6-dioxo-5-tridecylcyclohexa-1,4-dienylamino)butanoate
CAS No.:1600526-64-4
Molecular Formula:C₂₉H₄₉NO₅
Molecular Weight:491.712
Hs Code.:

Synonyms:butyl 4-(4-methoxy-2-methyl-3,6-dioxo-5-tridecylcyclohexa-1,4-dienylamino)butanoate

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Chemical Property of butyl 4-(4-methoxy-2-methyl-3,6-dioxo-5-tridecylcyclohexa-1,4-dienylamino)butanoate

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Technology Process of butyl 4-(4-methoxy-2-methyl-3,6-dioxo-5-tridecylcyclohexa-1,4-dienylamino)butanoate

There total 6 articles about butyl 4-(4-methoxy-2-methyl-3,6-dioxo-5-tridecylcyclohexa-1,4-dienylamino)butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.0%

: 101372-88-7
C₈H₁₇NO₂*C₇H₈O₃S

: 2,5-dimethoxy-3-methyl-6-tridecylcyclohexa-2,5-diene-1,4-dione

: 1600526-64-4
butyl 4-(4-methoxy-2-methyl-3,6-dioxo-5-tridecylcyclohexa-1,4-dienylamino)butanoate

: 1600526-65-5
C₃₆H₆₂N₂O₆

Guidance literature:: With sodium hydrogencarbonate; In ethanol; for 27h;

Reference yield:

: 219144-65-7
1,2,4,5-tetramethoxy-3-tridecylbenzene

: 1600526-64-4
butyl 4-(4-methoxy-2-methyl-3,6-dioxo-5-tridecylcyclohexa-1,4-dienylamino)butanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / tetrahydrofuran; hexane / 2.08 h / -78 - 0 °C

1.2: 15 h / 20 °C

2.1: ammonium cerium (IV) nitrate / acetonitrile / 3.5 h / -7 - 20 °C

3.1: sodium hydrogencarbonate / ethanol / 27 h

With n-butyllithium; ammonium cerium (IV) nitrate; N,N,N,N,-tetramethylethylenediamine; sodium hydrogencarbonate; In tetrahydrofuran; ethanol; hexane; acetonitrile;

Reference yield:

: 4460-86-0,14374-62-0
asaraldehyde

: 1600526-64-4
butyl 4-(4-methoxy-2-methyl-3,6-dioxo-5-tridecylcyclohexa-1,4-dienylamino)butanoate

Guidance literature:: Multi-step reaction with 6 steps

1.1: dihydrogen peroxide; sulfuric acid / methanol / 2 h / 20 °C / Inert atmosphere; Reflux

2.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 - 20 °C / Inert atmosphere

2.2: 13 h / 20 °C

3.1: N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium / tetrahydrofuran; hexane / 2.08 h / -40 - 0 °C

3.2: 15 h / 0 - 20 °C / Inert atmosphere

4.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / tetrahydrofuran; hexane / 2.08 h / -78 - 0 °C

4.2: 15 h / 20 °C

5.1: ammonium cerium (IV) nitrate / acetonitrile / 3.5 h / -7 - 20 °C

6.1: sodium hydrogencarbonate / ethanol / 27 h

With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; ammonium cerium (IV) nitrate; N,N,N,N,-tetramethylethylenediamine; sulfuric acid; dihydrogen peroxide; sodium hydride; sodium hydrogencarbonate; In tetrahydrofuran; methanol; ethanol; hexane; N,N-dimethyl-formamide; acetonitrile;