Dimethyl 2-(4-chlorophenyl)-3-nitropropylphosphonate

Base Information

Chemical Name:Dimethyl 2-(4-chlorophenyl)-3-nitropropylphosphonate
CAS No.:124831-11-4
Molecular Formula:C₁₁H₁₅ClNO₅P
Molecular Weight:307.671
Hs Code.:

Synonyms:Dimethyl 2-(4-chlorophenyl)-3-nitropropylphosphonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Dimethyl 2-(4-chlorophenyl)-3-nitropropylphosphonate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
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MSDS Files:: SDS file from LookChem

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Technology Process of Dimethyl 2-(4-chlorophenyl)-3-nitropropylphosphonate

There total 1 articles about Dimethyl 2-(4-chlorophenyl)-3-nitropropylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 706-07-0,5153-70-8
1-chloro-4-(2-nitrovinyl)benzene

: 756-79-6
dimethyl methane phosphonate

: 124831-11-4
Dimethyl 2-(4-chlorophenyl)-3-nitropropylphosphonate

Guidance literature:: With lithium diisopropyl amide; Yield given. Multistep reaction; 1.) THF, -78 deg C, 1 h, 2.) -78 deg C -> room temp.;
DOI:10.1055/s-1989-27279

Reference yield:

: 124831-11-4
Dimethyl 2-(4-chlorophenyl)-3-nitropropylphosphonate

: 124831-12-5
Dimethyl 3-amino-2-(4-chlorophenyl)propylphosphonate

Guidance literature:: With ammonium hydroxide; hydrogen; nickel; In ethanol; under 750.06 Torr; Yield given;
DOI:10.1055/s-1989-27279

Reference yield:

: 124831-11-4
Dimethyl 2-(4-chlorophenyl)-3-nitropropylphosphonate

: 114012-12-3,108351-35-5
phaclofen

Guidance literature:: Multi-step reaction with 2 steps

1: H₂, 8percent NH₃ / Raney Nickel / ethanol / 750.06 Torr

2: 61 percent / 36percent aq. HCl / 15 h / Heating

With hydrogenchloride; ammonium hydroxide; hydrogen; nickel; In ethanol;
DOI:10.1055/s-1989-27279