C₆₇H₈₆O₁₀SeSi₂

Base Information

Chemical Name:C₆₇H₈₆O₁₀SeSi₂
CAS No.:1265446-53-4
Molecular Formula:C₆₇H₈₆O₁₀SeSi₂
Molecular Weight:1186.54
Hs Code.:

C<sub>67</sub>H<sub>86</sub>O<sub>10</sub>SeSi<sub>2</sub>

Synonyms:C₆₇H₈₆O₁₀SeSi₂

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Chemical Property of C₆₇H₈₆O₁₀SeSi₂

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Technology Process of C₆₇H₈₆O₁₀SeSi₂

There total 1 articles about C₆₇H₈₆O₁₀SeSi₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 1666-13-3
diphenyl diselenide

: 1265446-50-1
C₆₃H₈₄O₁₂Si₂

: 1265446-53-4
C₆₇H₈₆O₁₀SeSi₂

Guidance literature:: diphenyl diselenide; With diisobutylaluminium hydride; In hexane; at 20 ℃; for 1h;

C₆₃H₈₄O₁₂Si₂; In hexane; dichloromethane; at 0 ℃; for 0.5h;
DOI:10.1021/np100729d

Reference yield: 60.0%

: 1265446-53-4
C₆₇H₈₆O₁₀SeSi₂

: 1265446-57-8
C₆₁H₇₂O₁₀SeSi

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at -30 - 0 ℃; for 2h;
DOI:10.1021/np100729d

Reference yield:

: 1265446-53-4
C₆₇H₈₆O₁₀SeSi₂

: C₅₇H₆₈O₁₁Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / -30 - 0 °C

2.1: methyllithium / tetrahydrofuran; diethyl ether / -78 - 20 °C

2.2: Inert atmosphere

3.1: triethyl borane; tri-n-butyl-tin hydride / tetrahydrofuran; toluene / 5 h / -40 - -15 °C / in air

4.1: pyridine; trifluoroacetic anhydride / acetonitrile / 7 h / 0 °C

With pyridine; triethyl borane; tetrabutyl ammonium fluoride; methyllithium; tri-n-butyl-tin hydride; trifluoroacetic anhydride; In tetrahydrofuran; diethyl ether; toluene; acetonitrile; 4.1: Pummerer reaction / 4.2: Pummerer reaction;
DOI:10.1021/np100729d