Imidazo[4,5-c]pyrazole-5(1H)-thione, 4,6-dihydro-1,3-dimethyl-

Base Information

Chemical Name:Imidazo[4,5-c]pyrazole-5(1H)-thione, 4,6-dihydro-1,3-dimethyl-
CAS No.:251989-15-8
Molecular Formula:C₆H₈N₄S
Molecular Weight:168.222
Hs Code.:
Mol file:251989-15-8.mol

Synonyms:Imidazo[4,5-c]pyrazole-5(1H)-thione, 4,6-dihydro-1,3-dimethyl-

Suppliers and Price of Imidazo[4,5-c]pyrazole-5(1H)-thione, 4,6-dihydro-1,3-dimethyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

AccelPharmtech
4,6-dihydro-1,3-dimethyl-Imidazo[4,5-c]pyrazole-5(1H)-thione 97.00%
1G
$ 1890.00

Total 2 raw suppliers

Chemical Property of Imidazo[4,5-c]pyrazole-5(1H)-thione, 4,6-dihydro-1,3-dimethyl-

Chemical Property:

Boiling Point:304.9±44.0 °C(Predicted)
PKA:11.36±0.20(Predicted)
PSA：81.49000
Density:1.61±0.1 g/cm3(Predicted)
LogP:1.26740

Purity/Quality:

99% ^*data from raw suppliers

4,6-dihydro-1,3-dimethyl-Imidazo[4,5-c]pyrazole-5(1H)-thione 97.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Imidazo[4,5-c]pyrazole-5(1H)-thione, 4,6-dihydro-1,3-dimethyl-

There total 3 articles about Imidazo[4,5-c]pyrazole-5(1H)-thione, 4,6-dihydro-1,3-dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 251989-08-9
1,3-dimethyl-4-isothiocyanato-1H-pyrazol-5-ylamine

: 251989-15-8
1,3-dimethyl-4,6-dihydro-1H-imidazo[4,5-c]pyrazole-5-thione

Guidance literature:: In pyridine; for 1h; Heating;
DOI:10.1002/(SICI)1521-4184(199910)332:10<337::AID-ARDP337>3.0.CO;2-P

Reference yield:

: 58663-94-8
1,3-dimethyl-4-nitroso-5-aminopyrazole

: 251989-15-8
1,3-dimethyl-4,6-dihydro-1H-imidazo[4,5-c]pyrazole-5-thione

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent N₂H₄*H₂O / 5 percent Pd-C / methanol / 0.08 h / Heating

2: H₂O / 2 h / 20 °C

3: 84 percent / pyridine / 1 h / Heating

With hydrazine hydrate; palladium on activated charcoal; In pyridine; methanol; water; 1: Reduction / 2: Condensation / 3: Cyclization;
DOI:10.1002/(SICI)1521-4184(199910)332:10<337::AID-ARDP337>3.0.CO;2-P

Reference yield:

: 96886-30-5
4,5-diamino-3-methyl-1-methyl-1H-pyrazole

: 251989-15-8
1,3-dimethyl-4,6-dihydro-1H-imidazo[4,5-c]pyrazole-5-thione

Guidance literature:: Multi-step reaction with 2 steps

1: H₂O / 2 h / 20 °C

2: 84 percent / pyridine / 1 h / Heating

In pyridine; water; 1: Condensation / 2: Cyclization;
DOI:10.1002/(SICI)1521-4184(199910)332:10<337::AID-ARDP337>3.0.CO;2-P