C₂₂H₁₁O₆Br₂F

Base Information

Chemical Name:C₂₂H₁₁O₆Br₂F
CAS No.:463927-70-0
Molecular Formula:C₂₂H₁₁Br₂FO₆
Molecular Weight:550.132
Hs Code.:

C<sub>22</sub>H<sub>11</sub>O<sub>6</sub>Br<sub>2</sub>F

Synonyms:C₂₂H₁₁O₆Br₂F

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Chemical Property of C₂₂H₁₁O₆Br₂F

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Technology Process of C₂₂H₁₁O₆Br₂F

There total 7 articles about C₂₂H₁₁O₆Br₂F which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 463927-69-7
C₂₄H₁₅O₆Br₂F

: 463927-70-0
C₂₂H₁₁O₆Br₂F

Guidance literature:: With sodium hydroxide; In ethanol; at 20 ℃;
DOI:10.1016/j.bmcl.2007.04.085

Reference yield:

: 672-13-9
2-hydroxy-5-methoxybenzaldehyde

: 463927-70-0
C₂₂H₁₁O₆Br₂F

Guidance literature:: Multi-step reaction with 7 steps

1: 33 percent / K₂CO₃ / dimethylformamide / 80 °C

2: 39 percent / BBr₃ / CH₂Cl₂ / 20 °C

3: 21 percent / Br₂; acetic acid / 50 °C

4: 20 percent / Cu bronze; NEt₃ / CH₂Cl₂ / 16 h / 0 - 20 °C

5: 46 percent / TiCl₄ / CH₂Cl₂ / 20 °C

6: 72 percent / AlCl₃; EtSH / CH₂Cl₂ / 20 °C

7: 84 percent / NaOH / ethanol / 20 °C

With sodium hydroxide; aluminium trichloride; copper bronze; bromine; boron tribromide; titanium tetrachloride; potassium carbonate; acetic acid; triethylamine; ethanethiol; In ethanol; dichloromethane; N,N-dimethyl-formamide; 5: Friedel-Crafts acylation;
DOI:10.1016/j.bmcl.2007.04.085

Reference yield:

: 99370-68-0
5-hydroxy-2-benzofuran-carboxylic acid ethyl ester

: 463927-70-0
C₂₂H₁₁O₆Br₂F

Guidance literature:: Multi-step reaction with 5 steps

1: 21 percent / Br₂; acetic acid / 50 °C

2: 20 percent / Cu bronze; NEt₃ / CH₂Cl₂ / 16 h / 0 - 20 °C

3: 46 percent / TiCl₄ / CH₂Cl₂ / 20 °C

4: 72 percent / AlCl₃; EtSH / CH₂Cl₂ / 20 °C

5: 84 percent / NaOH / ethanol / 20 °C

With sodium hydroxide; aluminium trichloride; copper bronze; bromine; titanium tetrachloride; acetic acid; triethylamine; ethanethiol; In ethanol; dichloromethane; 3: Friedel-Crafts acylation;
DOI:10.1016/j.bmcl.2007.04.085