p-nitrophenyl 2,4,6-tri-O-acetyl-3-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-α-D-mannopyranoside

Base Information

Chemical Name:p-nitrophenyl 2,4,6-tri-O-acetyl-3-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-α-D-mannopyranoside
CAS No.:105600-45-1
Molecular Formula:C₃₂H₃₉NO₂₀
Molecular Weight:757.656
Hs Code.:

Synonyms:p-nitrophenyl 2,4,6-tri-O-acetyl-3-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-α-D-mannopyranoside

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Chemical Property of p-nitrophenyl 2,4,6-tri-O-acetyl-3-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-α-D-mannopyranoside

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Technology Process of p-nitrophenyl 2,4,6-tri-O-acetyl-3-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-α-D-mannopyranoside

There total 5 articles about p-nitrophenyl 2,4,6-tri-O-acetyl-3-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 105600-44-0
p-nitrophenyl 2,4,6-tri-O-acetyl-α-D-mannopyranoside

: 13242-53-0
acetobromomannose

: 105600-45-1
p-nitrophenyl 2,4,6-tri-O-acetyl-3-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-α-D-mannopyranoside

Guidance literature:: With 4 A molecular sieve; mercury(II) cyanide; mercury dibromide; In acetonitrile; Ambient temperature;
DOI:10.1016/S0008-6215(00)90315-X

Reference yield:

: 105600-43-9
4-nitrophenyl 4,6-di-O-acetyl-α-D-mannopyranoside

: 105600-45-1
p-nitrophenyl 2,4,6-tri-O-acetyl-3-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: p-toluenesulfonic acid monohydrate / benzene / 1 h / Ambient temperature

2: 1.41 g / 80percent acetic acid / 0.25 h / Ambient temperature

3: 76 percent / mercuric bromide, mercuric cyanide, molecular sieves 4A / acetonitrile / Ambient temperature

With 4 A molecular sieve; mercury(II) cyanide; toluene-4-sulfonic acid; acetic acid; mercury dibromide; In acetonitrile; benzene;
DOI:10.1016/S0008-6215(00)90315-X

Reference yield:

: 80264-82-0
p-nitrophenyl 2,3-O-isopropylidene-α-D-mannopyranoside

: 105600-45-1
p-nitrophenyl 2,4,6-tri-O-acetyl-3-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 87 percent / pyridine

2: 88 percent / trifluoroacetic acid, water / 1 h / Ambient temperature

3: p-toluenesulfonic acid monohydrate / benzene / 1 h / Ambient temperature

4: 1.41 g / 80percent acetic acid / 0.25 h / Ambient temperature

5: 76 percent / mercuric bromide, mercuric cyanide, molecular sieves 4A / acetonitrile / Ambient temperature

With pyridine; 4 A molecular sieve; water; mercury(II) cyanide; toluene-4-sulfonic acid; acetic acid; trifluoroacetic acid; mercury dibromide; In acetonitrile; benzene;
DOI:10.1016/S0008-6215(00)90315-X