N-<5-anilino-3-chloro-2,4-(propane-1',3'-diyl)-2,4-pentadien-1-ylidene>anilinium chloride

Base Information

• Chemical Name: N-<5-anilino-3-chloro-2,4-(propane-1',3'-diyl)-2,4-pentadien-1-ylidene>anilinium chloride
• CAS No.: 195382-10-6
• Molecular Formula: C₂₀H₁₉ClN₂*ClH
• Molecular Weight: 359.298
• Mol file: 195382-10-6.mol

Synonyms:N-<5-anilino-3-chloro-2,4-(propane-1',3'-diyl)-2,4-pentadien-1-ylidene>anilinium chloride

Chemical Property of N-<5-anilino-3-chloro-2,4-(propane-1',3'-diyl)-2,4-pentadien-1-ylidene>anilinium chloride

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-<5-anilino-3-chloro-2,4-(propane-1',3'-diyl)-2,4-pentadien-1-ylidene>anilinium chloride

There total 5 articles about N-<5-anilino-3-chloro-2,4-(propane-1',3'-diyl)-2,4-pentadien-1-ylidene>anilinium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) + N,N-dimethyl-formamide (68-12-2,33513-42-7) + aniline (62-53-3) → N-<5-anilino-3-chloro-2,4-(propane-1',3'-diyl)-2,4-pentadien-1-ylidene>anilinium chloride (195382-10-6)

Guidance literature:

N,N-dimethyl-formamide; With trichlorophosphate; at 0 ℃; for 0.5h;

cyclohexanone; for 1h; Reflux;

aniline; Further stages;

DOI:10.1016/j.dyepig.2013.04.037

Reference yield: 40.1%

cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) + aniline (62-53-3) + N-methyl-N-phenylformamide (93-61-8) → N-<5-anilino-3-chloro-2,4-(propane-1',3'-diyl)-2,4-pentadien-1-ylidene>anilinium chloride (195382-10-6)

Guidance literature:

N-methyl-N-phenylformamide; With trichlorophosphate; at 0 ℃; for 0.5h; Inert atmosphere;

cyclohexanone; for 1h; Inert atmosphere; Reflux;

aniline; Further stages;

DOI:10.1016/j.dyepig.2013.05.001

Reference yield: 28.0%

cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) → N-<5-anilino-3-chloro-2,4-(propane-1',3'-diyl)-2,4-pentadien-1-ylidene>anilinium chloride (195382-10-6)

Guidance literature:

upstream raw materials:

cyclohexanone

aniline

N-methyl-N-phenylformamide

N,N-dimethyl-formamide

Downstream raw materials:

2-<4'diphenylphosphino-7'-(1''-ethyl-3'',3''-dimethylindolin-2''-ylidene)-3',5'-(propane-1''',3'''-diyl)-1',3',5'-heptatrien-1'-yl>-1-ethyl-3,3-dimethylindolinium iodide