O-[6-(3-decyloxyphenyloxy)hexyl]-4,4'-bis(methoxycarbonylphenyl)methanone oxime

Base Information

Chemical Name:O-[6-(3-decyloxyphenyloxy)hexyl]-4,4'-bis(methoxycarbonylphenyl)methanone oxime
CAS No.:912806-45-2
Molecular Formula:C₃₉H₅₁NO₇
Molecular Weight:645.836
Hs Code.:

Synonyms:O-[6-(3-decyloxyphenyloxy)hexyl]-4,4'-bis(methoxycarbonylphenyl)methanone oxime

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Chemical Property of O-[6-(3-decyloxyphenyloxy)hexyl]-4,4'-bis(methoxycarbonylphenyl)methanone oxime

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Technology Process of O-[6-(3-decyloxyphenyloxy)hexyl]-4,4'-bis(methoxycarbonylphenyl)methanone oxime

There total 8 articles about O-[6-(3-decyloxyphenyloxy)hexyl]-4,4'-bis(methoxycarbonylphenyl)methanone oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 875210-87-0
4,4'-bis(methoxycarbonylphenyl)methanone oxime

: 912806-38-3
1-(6-bromohexyloxy)-3-decyloxybenzene

: 912806-45-2
O-[6-(3-decyloxyphenyloxy)hexyl]-4,4'-bis(methoxycarbonylphenyl)methanone oxime

Guidance literature:: 4,4'-bis(methoxycarbonylphenyl)methanone oxime; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.25h;

1-(6-bromohexyloxy)-3-decyloxybenzene; With tetra-(n-butyl)ammonium iodide; In N,N-dimethyl-formamide; at 20 ℃; for 1h;
DOI:10.1021/jm060468y

Reference yield:

: 112-29-8
1-bromo dodecane

: 912806-45-2
O-[6-(3-decyloxyphenyloxy)hexyl]-4,4'-bis(methoxycarbonylphenyl)methanone oxime

Guidance literature:: Multi-step reaction with 3 steps

1.1: 93 percent / aq. potassium hydroxide / 3 h / Heating

2.1: 60 percent / potassium carbonate / cyclohexanone / 16 h / Heating

3.1: sodium hydride / dimethylformamide / 0.25 h / 0 °C

3.2: 62 percent / n-Bu₄NI / dimethylformamide / 1 h / 20 °C

With potassium hydroxide; sodium hydride; potassium carbonate; In cyclohexanone; N,N-dimethyl-formamide;
DOI:10.1021/jm060468y

Reference yield:

: 1233-73-4
Benzophenone-4,4'-dicarboxylic acid dimethyl ester

: 912806-45-2
O-[6-(3-decyloxyphenyloxy)hexyl]-4,4'-bis(methoxycarbonylphenyl)methanone oxime

Guidance literature:: Multi-step reaction with 2 steps

1.1: 88 percent / HCl*H₂NOH; sodium acetate / ethanol / 24 h / Heating

2.1: sodium hydride / dimethylformamide / 0.25 h / 0 °C

2.2: 62 percent / n-Bu₄NI / dimethylformamide / 1 h / 20 °C

With hydroxylamine hydrochloride; sodium acetate; sodium hydride; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm060468y