Technology Process of O-[6-(3-decyloxyphenyloxy)hexyl]-4,4'-bis(methoxycarbonylphenyl)methanone oxime
There total 8 articles about O-[6-(3-decyloxyphenyloxy)hexyl]-4,4'-bis(methoxycarbonylphenyl)methanone oxime which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
4,4'-bis(methoxycarbonylphenyl)methanone oxime;
With
sodium hydride;
In
N,N-dimethyl-formamide;
at 0 ℃;
for 0.25h;
1-(6-bromohexyloxy)-3-decyloxybenzene;
With
tetra-(n-butyl)ammonium iodide;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 1h;
DOI:10.1021/jm060468y
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 93 percent / aq. potassium hydroxide / 3 h / Heating
2.1: 60 percent / potassium carbonate / cyclohexanone / 16 h / Heating
3.1: sodium hydride / dimethylformamide / 0.25 h / 0 °C
3.2: 62 percent / n-Bu4NI / dimethylformamide / 1 h / 20 °C
With
potassium hydroxide; sodium hydride; potassium carbonate;
In
cyclohexanone; N,N-dimethyl-formamide;
DOI:10.1021/jm060468y
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: 88 percent / HCl*H2NOH; sodium acetate / ethanol / 24 h / Heating
2.1: sodium hydride / dimethylformamide / 0.25 h / 0 °C
2.2: 62 percent / n-Bu4NI / dimethylformamide / 1 h / 20 °C
With
hydroxylamine hydrochloride; sodium acetate; sodium hydride;
In
ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm060468y
