(S)-tert-butyl [1-(3,4-dichlorophenyl)-4-methoxy-4-oxobutyl]-1H-indole-1-carboxylate

Base Information

• Chemical Name: (S)-tert-butyl [1-(3,4-dichlorophenyl)-4-methoxy-4-oxobutyl]-1H-indole-1-carboxylate
• CAS No.: 1097642-33-5
• Molecular Formula: C₂₄H₂₅Cl₂NO₄
• Molecular Weight: 462.373

Synonyms:(S)-tert-butyl [1-(3,4-dichlorophenyl)-4-methoxy-4-oxobutyl]-1H-indole-1-carboxylate

Chemical Property of (S)-tert-butyl [1-(3,4-dichlorophenyl)-4-methoxy-4-oxobutyl]-1H-indole-1-carboxylate

Chemical Property:

Purity/Quality:

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Technology Process of (S)-tert-butyl [1-(3,4-dichlorophenyl)-4-methoxy-4-oxobutyl]-1H-indole-1-carboxylate

There total 1 articles about (S)-tert-butyl [1-(3,4-dichlorophenyl)-4-methoxy-4-oxobutyl]-1H-indole-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

(S,E)-tert-butyl 4-[1-(3,4-dichlorophenyl)-4-methoxy-4-oxobut-2-enyl]-1H-indole-1-carboxylate (877170-85-9) → (S)-tert-butyl [1-(3,4-dichlorophenyl)-4-methoxy-4-oxobutyl]-1H-indole-1-carboxylate (1097642-33-5)

Guidance literature:

With Wilkinson's catalyst; hydrogen; In ethanol; under 2327.23 Torr; optical yield given as %ee;

DOI:10.1016/j.bmcl.2008.11.022

Reference yield: 97.0%

(S)-tert-butyl [1-(3,4-dichlorophenyl)-4-methoxy-4-oxobutyl]-1H-indole-1-carboxylate (1097642-33-5) → (R)-4-[1-(tert-butoxycarbonyl)-1H-indol-4-yl]-4-(3,4-dichlorophenyl)butanoic acid

Guidance literature:

With lithium hydroxide monohydrate; water; In tetrahydrofuran; at 20 ℃;

DOI:10.1016/j.bmcl.2008.11.022

Reference yield: 97.0%

(S)-tert-butyl [1-(3,4-dichlorophenyl)-4-methoxy-4-oxobutyl]-1H-indole-1-carboxylate (1097642-33-5) → (S)-tert-butyl 4-[1-(3,4-dichlorophenyl)-4-hydroxybutyl]-1H-indole-1-carboxylate

Guidance literature:

With diisobutylaluminium hydride; In tetrahydrofuran; at 20 ℃; for 3h; Inert atmosphere;

DOI:10.1016/j.bmcl.2008.11.022

upstream raw materials:

(S,E)-tert-butyl 4-[1-(3,4-dichlorophenyl)-4-methoxy-4-oxobut-2-enyl]-1H-indole-1-carboxylate

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