(2R,3R)-3-benzyloxy-1,2-pentanediol

Base Information

Chemical Name:(2R,3R)-3-benzyloxy-1,2-pentanediol
CAS No.:99944-96-4
Molecular Formula:C₁₂H₁₈O₃
Molecular Weight:210.273
Hs Code.:

Synonyms:(2R,3R)-3-benzyloxy-1,2-pentanediol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,3R)-3-benzyloxy-1,2-pentanediol

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Technology Process of (2R,3R)-3-benzyloxy-1,2-pentanediol

There total 4 articles about (2R,3R)-3-benzyloxy-1,2-pentanediol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1140786-15-7
(2R,3R)-3-benzyloxy-1,2-cyclohexylidenedioxypentane

: 99944-96-4
(2R,3R)-3-benzyloxy-1,2-pentanediol

Guidance literature:: With copper(II) chloride monohydrate; In methanol; at 50 ℃; for 4h;
DOI:10.1002/chem.200801603

Reference yield: 82.0%

: (2R)-3-benzyloxy-1,2-cyclohexylidenedioxypentane

: 99838-62-7,99944-96-4,108740-35-8
(2R,3RS)-3-O-benzylpentane-1,2,3-triol

Guidance literature:: With toluene-4-sulfonic acid; In methanol; at 50 ℃; for 8h; Inert atmosphere;
DOI:10.1002/hlca.201400344

Reference yield:

: 943154-77-6
(2R,3S/R)-1,2-(cyclohexylidenedioxy)pentan-3-ol

: 99838-62-7,99944-96-4,108740-35-8
(2R,3RS)-3-O-benzylpentane-1,2,3-triol

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran / 0.33 h / 0 °C / Inert atmosphere

1.2: Inert atmosphere

2.1: toluene-4-sulfonic acid / methanol / 8 h / 50 °C / Inert atmosphere

With sodium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; methanol;
DOI:10.1002/hlca.201400344