N-acetyl-5-[2',3'-O-diacetyl-β-D-ribofuranosyl]-3-nitro-6-[2-(4-nitrophenyl)ethoxy]-2-pyridinamine

Base Information

Chemical Name:N-acetyl-5-[2',3'-O-diacetyl-β-D-ribofuranosyl]-3-nitro-6-[2-(4-nitrophenyl)ethoxy]-2-pyridinamine
CAS No.:1582314-24-6
Molecular Formula:C₂₄H₂₆N₄O₁₂
Molecular Weight:562.49
Hs Code.:

Synonyms:N-acetyl-5-[2',3'-O-diacetyl-β-D-ribofuranosyl]-3-nitro-6-[2-(4-nitrophenyl)ethoxy]-2-pyridinamine

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Chemical Property of N-acetyl-5-[2',3'-O-diacetyl-β-D-ribofuranosyl]-3-nitro-6-[2-(4-nitrophenyl)ethoxy]-2-pyridinamine

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Technology Process of N-acetyl-5-[2',3'-O-diacetyl-β-D-ribofuranosyl]-3-nitro-6-[2-(4-nitrophenyl)ethoxy]-2-pyridinamine

There total 7 articles about N-acetyl-5-[2',3'-O-diacetyl-β-D-ribofuranosyl]-3-nitro-6-[2-(4-nitrophenyl)ethoxy]-2-pyridinamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1582314-30-4
C₄₅H₄₄N₄O₁₄

: 1582314-24-6
N-acetyl-5-[2',3'-O-diacetyl-β-D-ribofuranosyl]-3-nitro-6-[2-(4-nitrophenyl)ethoxy]-2-pyridinamine

Guidance literature:: With dichloro-acetic acid; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1021/jo402665d

Reference yield:

: 1582314-29-1
C₄₁H₃₈N₄O₁₁

: 1582314-24-6
N-acetyl-5-[2',3'-O-diacetyl-β-D-ribofuranosyl]-3-nitro-6-[2-(4-nitrophenyl)ethoxy]-2-pyridinamine

Guidance literature:: Multi-step reaction with 6 steps

1: Dess-Martin periodane / dichloromethane / 4 h / 20 °C

2: trifluoroacetic acid / dichloromethane / 3 h / 20 °C

3: acetic acid; sodium tris(acetoxy)borohydride / acetonitrile / 1 h / 0 °C

4: dmap; triethylamine / dichloromethane / 1 h / 20 °C

5: dmap; pyridine / dichloromethane / 3 h / 20 °C

6: dichloro-acetic acid / dichloromethane / 1 h / 20 °C

With pyridine; dichloro-acetic acid; dmap; sodium tris(acetoxy)borohydride; Dess-Martin periodane; acetic acid; triethylamine; trifluoroacetic acid; In dichloromethane; acetonitrile;
DOI:10.1021/jo402665d

Reference yield:

: 1582314-22-4
5-(2'-O-acetyl-β-D-ribofuranosyl)-3-nitro-6-[2-(4-nitrophenyl)ethoxy]-2-pyridinamine

: 1582314-24-6
N-acetyl-5-[2',3'-O-diacetyl-β-D-ribofuranosyl]-3-nitro-6-[2-(4-nitrophenyl)ethoxy]-2-pyridinamine

Guidance literature:: Multi-step reaction with 3 steps

1: dmap; triethylamine / dichloromethane / 1 h / 20 °C

2: dmap; pyridine / dichloromethane / 3 h / 20 °C

3: dichloro-acetic acid / dichloromethane / 1 h / 20 °C

With pyridine; dichloro-acetic acid; dmap; triethylamine; In dichloromethane;
DOI:10.1021/jo402665d