phenyl 3-O-acetyl-2,4-diazido-2,4,6-trideoxy-1-thio-β-D-galactopyranoside

Base Information

Chemical Name:phenyl 3-O-acetyl-2,4-diazido-2,4,6-trideoxy-1-thio-β-D-galactopyranoside
CAS No.:1432492-24-4
Molecular Formula:C₁₉H₁₈N₆O₃S
Molecular Weight:410.456
Hs Code.:

Synonyms:phenyl 3-O-acetyl-2,4-diazido-2,4,6-trideoxy-1-thio-β-D-galactopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenyl 3-O-acetyl-2,4-diazido-2,4,6-trideoxy-1-thio-β-D-galactopyranoside

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Technology Process of phenyl 3-O-acetyl-2,4-diazido-2,4,6-trideoxy-1-thio-β-D-galactopyranoside

There total 6 articles about phenyl 3-O-acetyl-2,4-diazido-2,4,6-trideoxy-1-thio-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: C₂₁H₁₈F₆O₉S₃

: 1432492-24-4
phenyl 3-O-acetyl-2,4-diazido-2,4,6-trideoxy-1-thio-β-D-galactopyranoside

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1021/acschembio.6b00790

Reference yield:

: 1432492-17-5
phenyl 3-O-benzoyl-6-deoxy-1-thio-β-D-mannopyranoside

: 1432492-24-4
phenyl 3-O-acetyl-2,4-diazido-2,4,6-trideoxy-1-thio-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; trifluoromethylsulfonic anhydride / dichloromethane / 2 h / -10 - 10 °C / Inert atmosphere

2: sodium azide / N,N-dimethyl-formamide / 8 h / 20 °C / Inert atmosphere

With pyridine; sodium azide; trifluoromethylsulfonic anhydride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c3ob40615f

Reference yield:

: 1432492-21-1
phenyl 6-O-tosyloxy-1-thio-β-D-mannopyranoside

: 1432492-24-4
phenyl 3-O-acetyl-2,4-diazido-2,4,6-trideoxy-1-thio-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 - 80 °C / Inert atmosphere

2: dimethyltin dichloride; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 1 h / Inert atmosphere

3: pyridine / dichloromethane / 2 h / -10 - 10 °C / Inert atmosphere

4: sodium azide / N,N-dimethyl-formamide / 8 h / 20 °C / Inert atmosphere

With pyridine; lithium aluminium tetrahydride; sodium azide; dimethyltin dichloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c3ob40615f