N-[2-(3-benzyloxy-4-methoxy-phenyl)-ethyl]-2-(3-methoxy-phenyl)-acetamide

Base Information

Chemical Name:N-[2-(3-benzyloxy-4-methoxy-phenyl)-ethyl]-2-(3-methoxy-phenyl)-acetamide
CAS No.:1027233-46-0
Molecular Formula:C₂₅H₂₇NO₄
Molecular Weight:405.494
Hs Code.:

<i>N</i>-[2-(3-benzyloxy-4-methoxy-phenyl)-ethyl]-2-(3-methoxy-phenyl)-acetamide

Synonyms:N-[2-(3-benzyloxy-4-methoxy-phenyl)-ethyl]-2-(3-methoxy-phenyl)-acetamide

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Chemical Property of N-[2-(3-benzyloxy-4-methoxy-phenyl)-ethyl]-2-(3-methoxy-phenyl)-acetamide

Chemical Property:

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Technology Process of N-[2-(3-benzyloxy-4-methoxy-phenyl)-ethyl]-2-(3-methoxy-phenyl)-acetamide

There total 8 articles about N-[2-(3-benzyloxy-4-methoxy-phenyl)-ethyl]-2-(3-methoxy-phenyl)-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 36455-21-7
3-benzyloxy-4-methoxyphenylethylamine

: 6834-42-0
3-methoxyphenylacetic acid chloride

: 1027233-46-0
N-[2-(3-benzyloxy-4-methoxy-phenyl)-ethyl]-2-(3-methoxy-phenyl)-acetamide

Guidance literature:: With 5percent aq. NaOH; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1021/jm020831a

Reference yield:

: 621-59-0
isovanillin

: 1027233-46-0
N-[2-(3-benzyloxy-4-methoxy-phenyl)-ethyl]-2-(3-methoxy-phenyl)-acetamide

Guidance literature:: Multi-step reaction with 4 steps

1: 94 percent / K₂CO₃ / ethanol / 5 h / Heating

2: 88 percent / NH₄OAc; AcOH / 4 h / Heating

3: 63 percent / LiAlH₄ / diethyl ether; tetrahydrofuran / 2 h / Heating

4: 5percent aq. NaOH / CH₂Cl₂ / 2 h / 20 °C

With lithium aluminium tetrahydride; ammonium acetate; potassium carbonate; acetic acid; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; 4: Schotten-Baumann reaction;
DOI:10.1021/jm020831a

Reference yield:

: 6346-05-0
3-benzyloxy-4-methoxybenzaldehyde

: 1027233-46-0
N-[2-(3-benzyloxy-4-methoxy-phenyl)-ethyl]-2-(3-methoxy-phenyl)-acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / NH₄OAc; AcOH / 4 h / Heating

2: 63 percent / LiAlH₄ / diethyl ether; tetrahydrofuran / 2 h / Heating

3: 5percent aq. NaOH / CH₂Cl₂ / 2 h / 20 °C

With lithium aluminium tetrahydride; ammonium acetate; acetic acid; In tetrahydrofuran; diethyl ether; dichloromethane; 3: Schotten-Baumann reaction;
DOI:10.1021/jm020831a