tert-butyl N'-[4-(tert-butyldiphenylsilanyloxy)-5-chloro-2-(3,4,5-trifluorophenyl)pentanoyl]hydrazinecarboxylate

Base Information

Chemical Name:tert-butyl N'-[4-(tert-butyldiphenylsilanyloxy)-5-chloro-2-(3,4,5-trifluorophenyl)pentanoyl]hydrazinecarboxylate
CAS No.:1123192-16-4
Molecular Formula:C₃₂H₃₈ClF₃N₂O₄Si
Molecular Weight:635.198
Hs Code.:

Synonyms:tert-butyl N'-[4-(tert-butyldiphenylsilanyloxy)-5-chloro-2-(3,4,5-trifluorophenyl)pentanoyl]hydrazinecarboxylate

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Chemical Property of tert-butyl N'-[4-(tert-butyldiphenylsilanyloxy)-5-chloro-2-(3,4,5-trifluorophenyl)pentanoyl]hydrazinecarboxylate

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Technology Process of tert-butyl N'-[4-(tert-butyldiphenylsilanyloxy)-5-chloro-2-(3,4,5-trifluorophenyl)pentanoyl]hydrazinecarboxylate

There total 2 articles about tert-butyl N'-[4-(tert-butyldiphenylsilanyloxy)-5-chloro-2-(3,4,5-trifluorophenyl)pentanoyl]hydrazinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1123192-15-3
tert-butyl N'-[5-chloro-4-hydroxy-2-(3,4,5-trifluorophenyl)pentanoyl]hydrazinecarboxylate

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1123192-16-4
tert-butyl N'-[4-(tert-butyldiphenylsilanyloxy)-5-chloro-2-(3,4,5-trifluorophenyl)pentanoyl]hydrazinecarboxylate

Guidance literature:: With 1H-imidazole; dmap; In N,N-dimethyl-formamide; at 60 ℃; for 2h;

Reference yield:

: 288-32-4
1H-imidazole

: 1123192-15-3
tert-butyl N'-[5-chloro-4-hydroxy-2-(3,4,5-trifluorophenyl)pentanoyl]hydrazinecarboxylate

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1123192-16-4
tert-butyl N'-[4-(tert-butyldiphenylsilanyloxy)-5-chloro-2-(3,4,5-trifluorophenyl)pentanoyl]hydrazinecarboxylate

Guidance literature:: With dmap; ammonium chloride; In ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: ethyl (E)-3-[3-methoxy-4-(4-methyl-1H-imidazol-1-yl)phenyl]acrylimidate dihydrochloride

: 1123192-16-4
tert-butyl N'-[4-(tert-butyldiphenylsilanyloxy)-5-chloro-2-(3,4,5-trifluorophenyl)pentanoyl]hydrazinecarboxylate

: 1123192-17-5
6-(tert-butyldiphenylsilanyloxy)-2-((E)-2-[3-methoxy-4-(4-methyl-1H-imidazol-1-yl)phenyl]vinyl)-8-(3,4,5-trifluorophenyl)-5,6,7,8-tetrahydro-[1,2,4]triazolo[1,5-a]pyridine

Guidance literature:: tert-butyl N'-[4-(tert-butyldiphenylsilanyloxy)-5-chloro-2-(3,4,5-trifluorophenyl)pentanoyl]hydrazinecarboxylate; With trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃; for 2h;

ethyl (E)-3-[3-methoxy-4-(4-methyl-1H-imidazol-1-yl)phenyl]acrylimidate dihydrochloride; With triethylamine; In ethanol; at 80 ℃; for 12h;