methyl (2-methyl-1-phenylbut-3-en-2-yl) carbonate

Base Information

Chemical Name:methyl (2-methyl-1-phenylbut-3-en-2-yl) carbonate
CAS No.:1413935-00-8
Molecular Formula:C₁₃H₁₆O₃
Molecular Weight:220.268
Hs Code.:

Synonyms:methyl (2-methyl-1-phenylbut-3-en-2-yl) carbonate

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Chemical Property of methyl (2-methyl-1-phenylbut-3-en-2-yl) carbonate

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Technology Process of methyl (2-methyl-1-phenylbut-3-en-2-yl) carbonate

There total 1 articles about methyl (2-methyl-1-phenylbut-3-en-2-yl) carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 42548-91-4
2-Methyl-1-phenyl-3-buten-2-ol

: 79-22-1
methyl chloroformate

: 1413935-00-8
methyl (2-methyl-1-phenylbut-3-en-2-yl) carbonate

Guidance literature:: 2-Methyl-1-phenyl-3-buten-2-ol; With lithium hexamethyldisilazane; In tetrahydrofuran; at 0 ℃; for 0.5h; Inert atmosphere;

methyl chloroformate; In tetrahydrofuran; at 20 ℃; for 4h; Inert atmosphere;
DOI:10.1021/ja306602g

Reference yield: 83.0%

: 1413935-00-8
methyl (2-methyl-1-phenylbut-3-en-2-yl) carbonate

: 99808-99-8
(R,S)-α-[(tert-butyldimethylsilyl)oxy]-α-(phenyl)acetonitrile

: 1413934-91-4
2-benzyl-2-methyl-1-phenylbut-3-en-1-one

Guidance literature:: (R,S)-α-[(tert-butyldimethylsilyl)oxy]-α-(phenyl)acetonitrile; With lithium hexamethyldisilazane; In tetrahydrofuran; at -10 ℃; for 0.5h; Inert atmosphere;

methyl (2-methyl-1-phenylbut-3-en-2-yl) carbonate; With chloro(1,5-cyclooctadiene)rhodium(I) dimer; tris(2,4-di-tert-butylphenyl)phosphite; In tetrahydrofuran; at -10 ℃; for 16h; Inert atmosphere;

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at -10 - 20 ℃; regioselective reaction; Inert atmosphere;
DOI:10.1021/ja306602g

Reference yield:

: 1413935-00-8
methyl (2-methyl-1-phenylbut-3-en-2-yl) carbonate

: 78978-57-1
2-(tert-butyldimethylsilyl)acetonitrile

: C₁₉H₂₉NSi

Guidance literature:: 2-(tert-butyldimethylsilyl)acetonitrile; With triphenyl phosphite; bis(1,5-cyclooctadiene)rhodium(I) trifluoromethanesulfonate; lithium hexamethyldisilazane; In tetrahydrofuran; at 0 ℃; Inert atmosphere;

methyl (2-methyl-1-phenylbut-3-en-2-yl) carbonate; In tetrahydrofuran; at 0 - 20 ℃; for 16h; regioselective reaction; Inert atmosphere;
DOI:10.1021/jacs.0c02316