12-(2-{2-[2-(12-Hydroxy-dodecyloxy)-ethoxy]-ethoxy}-ethoxy)-dodecan-1-ol

Base Information

Chemical Name:12-(2-{2-[2-(12-Hydroxy-dodecyloxy)-ethoxy]-ethoxy}-ethoxy)-dodecan-1-ol
CAS No.:165191-84-4
Molecular Formula:C₃₀H₆₂O₆
Molecular Weight:518.819
Hs Code.:

Synonyms:12-(2-{2-[2-(12-Hydroxy-dodecyloxy)-ethoxy]-ethoxy}-ethoxy)-dodecan-1-ol

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Chemical Property of 12-(2-{2-[2-(12-Hydroxy-dodecyloxy)-ethoxy]-ethoxy}-ethoxy)-dodecan-1-ol

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Technology Process of 12-(2-{2-[2-(12-Hydroxy-dodecyloxy)-ethoxy]-ethoxy}-ethoxy)-dodecan-1-ol

There total 3 articles about 12-(2-{2-[2-(12-Hydroxy-dodecyloxy)-ethoxy]-ethoxy}-ethoxy)-dodecan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 16.0%

: 165191-83-3
C₄₀H₇₈O₈

: 165191-84-4,78336-31-9
12-(2-{2-[2-(12-Hydroxy-dodecyloxy)-ethoxy]-ethoxy}-ethoxy)-dodecan-1-ol

: 12-[2-(2-{2-[12-(Tetrahydro-pyran-2-yloxy)-dodecyloxy]-ethoxy}-ethoxy)-ethoxy]-dodecan-1-ol

Guidance literature:: With toluene-4-sulfonic acid; In methanol; water; at 60 ℃; for 8h;
DOI:10.1021/ja00134a011

Reference yield:

: 3344-77-2
12-bromododecanol

: 165191-84-4,78336-31-9
12-(2-{2-[2-(12-Hydroxy-dodecyloxy)-ethoxy]-ethoxy}-ethoxy)-dodecan-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / p-toluenesulfonic acid monohydrate / CH₂Cl₂ / 3.5 h / 0 °C

2: 17 percent / tetrabutylammonium sulfate, 50percent NaOH / H₂O / 24 h

3: 37 percent / p-toluenesulfonic acid monohydrate / methanol; H₂O / 8 h / 60 °C

With sodium hydroxide; toluene-4-sulfonic acid; tetrabutylammonium sulfate; In methanol; dichloromethane; water;
DOI:10.1021/ja00134a011

Reference yield:

: 112999-97-0,88517-92-4
2-[(12-bromododecyl)oxy]tetrahydro-2H-pyran

: 165191-84-4,78336-31-9
12-(2-{2-[2-(12-Hydroxy-dodecyloxy)-ethoxy]-ethoxy}-ethoxy)-dodecan-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 17 percent / tetrabutylammonium sulfate, 50percent NaOH / H₂O / 24 h

2: 37 percent / p-toluenesulfonic acid monohydrate / methanol; H₂O / 8 h / 60 °C

With sodium hydroxide; toluene-4-sulfonic acid; tetrabutylammonium sulfate; In methanol; water;
DOI:10.1021/ja00134a011