1-Allyl 7-ethyl 2-allyloxycarbonyl-2-[2-(4-cyanophenyl)ethyl]heptandioate

Base Information

Chemical Name:1-Allyl 7-ethyl 2-allyloxycarbonyl-2-[2-(4-cyanophenyl)ethyl]heptandioate
CAS No.:934753-48-7
Molecular Formula:C₂₅H₃₁NO₆
Molecular Weight:441.524
Hs Code.:

Synonyms:1-Allyl 7-ethyl 2-allyloxycarbonyl-2-[2-(4-cyanophenyl)ethyl]heptandioate

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Chemical Property of 1-Allyl 7-ethyl 2-allyloxycarbonyl-2-[2-(4-cyanophenyl)ethyl]heptandioate

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Technology Process of 1-Allyl 7-ethyl 2-allyloxycarbonyl-2-[2-(4-cyanophenyl)ethyl]heptandioate

There total 5 articles about 1-Allyl 7-ethyl 2-allyloxycarbonyl-2-[2-(4-cyanophenyl)ethyl]heptandioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

: 72054-56-9
4-(2-bromoethyl)benzonitrile

: 934753-47-6
1-allyl 7-ethyl 2-allyloxycarbonylheptanedioate

: 934753-48-7
1-Allyl 7-ethyl 2-allyloxycarbonyl-2-[2-(4-cyanophenyl)ethyl]heptandioate

Guidance literature:: 1-allyl 7-ethyl 2-allyloxycarbonylheptanedioate; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h;

4-(2-bromoethyl)benzonitrile; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h;

Reference yield:

: 1-(2-bromoethyl)-4-hydroxymethylbenzene

: 934753-48-7
1-Allyl 7-ethyl 2-allyloxycarbonyl-2-[2-(4-cyanophenyl)ethyl]heptandioate

Guidance literature:: Multi-step reaction with 3 steps

1.1: pyridinium chlorochromate / dichloromethane / 20 °C

2.1: formic acid; hydroxylamine hydrochloride / 2 h / Reflux

3.1: sodium hydride / N,N-dimethyl-formamide / 0 - 20 °C

3.2: 0 - 20 °C

With formic acid; hydroxylamine hydrochloride; sodium hydride; pyridinium chlorochromate; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 52062-92-7
4-(2-bromoethyl)benzoic acid

: 934753-48-7
1-Allyl 7-ethyl 2-allyloxycarbonyl-2-[2-(4-cyanophenyl)ethyl]heptandioate

Guidance literature:: Multi-step reaction with 4 steps

1.1: borane-THF / tetrahydrofuran / -10 - 20 °C

2.1: pyridinium chlorochromate / dichloromethane / 20 °C

3.1: formic acid; hydroxylamine hydrochloride / 2 h / Reflux

4.1: sodium hydride / N,N-dimethyl-formamide / 0 - 20 °C

4.2: 0 - 20 °C

With formic acid; borane-THF; hydroxylamine hydrochloride; sodium hydride; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;