4,10-Bis-[((S)-1-ethoxycarbonyl-2-phenyl-ethylcarbamoyl)-methyl]-1,4,7,10-tetraaza-cyclododecane-1,7-dicarboxylic acid dibenzyl ester

Base Information

Chemical Name:4,10-Bis-[((S)-1-ethoxycarbonyl-2-phenyl-ethylcarbamoyl)-methyl]-1,4,7,10-tetraaza-cyclododecane-1,7-dicarboxylic acid dibenzyl ester
CAS No.:914791-80-3
Molecular Formula:C₅₀H₆₂N₆O₁₀
Molecular Weight:907.076
Hs Code.:

Synonyms:4,10-Bis-[((S)-1-ethoxycarbonyl-2-phenyl-ethylcarbamoyl)-methyl]-1,4,7,10-tetraaza-cyclododecane-1,7-dicarboxylic acid dibenzyl ester

Suppliers and Price of 4,10-Bis-[((S)-1-ethoxycarbonyl-2-phenyl-ethylcarbamoyl)-methyl]-1,4,7,10-tetraaza-cyclododecane-1,7-dicarboxylic acid dibenzyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4,10-Bis-[((S)-1-ethoxycarbonyl-2-phenyl-ethylcarbamoyl)-methyl]-1,4,7,10-tetraaza-cyclododecane-1,7-dicarboxylic acid dibenzyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4,10-Bis-[((S)-1-ethoxycarbonyl-2-phenyl-ethylcarbamoyl)-methyl]-1,4,7,10-tetraaza-cyclododecane-1,7-dicarboxylic acid dibenzyl ester

There total 1 articles about 4,10-Bis-[((S)-1-ethoxycarbonyl-2-phenyl-ethylcarbamoyl)-methyl]-1,4,7,10-tetraaza-cyclododecane-1,7-dicarboxylic acid dibenzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 32132-71-1,76562-68-0
L-2-(2-bromo-acetylamino)-3-phenylpropionic acid ethyl ester

: 162148-45-0
1,4,7,10-tetraaza-cyclododecane-1,7-dicarboxylic acid dibenzyl ester

: 914791-80-3
4,10-Bis-[((S)-1-ethoxycarbonyl-2-phenyl-ethylcarbamoyl)-methyl]-1,4,7,10-tetraaza-cyclododecane-1,7-dicarboxylic acid dibenzyl ester

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1021/ja056303g

Reference yield:

: 914791-80-3
4,10-Bis-[((S)-1-ethoxycarbonyl-2-phenyl-ethylcarbamoyl)-methyl]-1,4,7,10-tetraaza-cyclododecane-1,7-dicarboxylic acid dibenzyl ester

: 881387-33-3
(S)-2-(2-{7-[((S)-1-Ethoxycarbonyl-2-phenyl-ethylcarbamoyl)-methyl]-1,4,7,10-tetraaza-cyclododec-1-yl}-acetylamino)-3-phenyl-propionic acid ethyl ester

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; at 20 ℃; for 96h; under 2068.59 Torr;
DOI:10.1021/ja056303g

Reference yield:

: 914791-80-3
4,10-Bis-[((S)-1-ethoxycarbonyl-2-phenyl-ethylcarbamoyl)-methyl]-1,4,7,10-tetraaza-cyclododecane-1,7-dicarboxylic acid dibenzyl ester

: 881387-34-4
2-{2-[7-[(1-ethoxycarbonyl-2-phenyl-ethylcarbamoyl)-methyl]-4-(5-oxo-5H-thiochromeno[2,3-b]pyridin-2-ylmethyl)-1,4,7,10tetraaza-cyclododec-1-yl]-acetylamino}-3-phenyl-propionic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 2.7 g / H₂ / Pd/C / ethanol / 96 h / 20 °C / 2068.59 Torr

2: 34 percent / K₂CO₃ / acetonitrile / 48 h / 20 °C

With hydrogen; potassium carbonate; palladium on activated charcoal; In ethanol; acetonitrile;
DOI:10.1021/ja056303g