C₃₀H₄₀O₂Si

Base Information

• Chemical Name: C₃₀H₄₀O₂Si
• CAS No.: 1361130-18-8
• Molecular Formula: C₃₀H₄₀O₂Si
• Molecular Weight: 460.732
• Mol file: 1361130-18-8.mol

Synonyms:C₃₀H₄₀O₂Si

Chemical Property of C₃₀H₄₀O₂Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₃₀H₄₀O₂Si

There total 1 articles about C₃₀H₄₀O₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

trityl chloride (76-83-5) + (3R)-4-(tert-butyldimethylsilanyloxy)-3-methylbutan-1-ol (147915-55-7) → C30H40O2Si (1361130-18-8)

Guidance literature:

With dmap; triethylamine; In dichloromethane; at 0 - 20 ℃; for 3h;

DOI:10.1021/ol300182r

Reference yield: 100.0%

C30H40O2Si (1361130-18-8) → C24H26O2 (1361130-19-9)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 - 20 ℃; for 5h;

DOI:10.1021/ol300182r

Reference yield:

C30H40O2Si (1361130-18-8) → C24H24O2 (1361130-20-2)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 5 h / 0 - 20 °C

2: Dess-Martin periodane / dichloromethane / 5 h / 0 °C

With tetrabutyl ammonium fluoride; Dess-Martin periodane; In tetrahydrofuran; dichloromethane; 2: Dess-Martin oxidation;

DOI:10.1021/ol300182r

upstream raw materials:

trityl chloride

(3R)-4-(tert-butyldimethylsilanyloxy)-3-methylbutan-1-ol

Downstream raw materials:

C₂₄H₂₆O₂

C₂₄H₂₄O₂

C₂₈H₃₂O₂

C₃₀H₃₄O₃