Di(tert-butyl)-N-(3-(<(E)-3-(4-hydroxyphenyl)prop-2-enoyl>amino)propyl)-N,N'-(butan-1,4-diyl)bis

Base Information

• Chemical Name: Di(tert-butyl)-N-(3-(<(E)-3-(4-hydroxyphenyl)prop-2-enoyl>amino)propyl)-N,N'-(butan-1,4-diyl)bis
• CAS No.: 69089-01-6
• Molecular Formula: C₂₆H₄₁N₃O₆
• Molecular Weight: 491.628

Synonyms:Di(tert-butyl)-N-(3-(<(E)-3-(4-hydroxyphenyl)prop-2-enoyl>amino)propyl)-N,N'-(butan-1,4-diyl)bis

Chemical Property of Di(tert-butyl)-N-(3-(<(E)-3-(4-hydroxyphenyl)prop-2-enoyl>amino)propyl)-N,N'-(butan-1,4-diyl)bis

Chemical Property:

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Technology Process of Di(tert-butyl)-N-(3-(<(E)-3-(4-hydroxyphenyl)prop-2-enoyl>amino)propyl)-N,N'-(butan-1,4-diyl)bis

There total 15 articles about Di(tert-butyl)-N-(3-(<(E)-3-(4-hydroxyphenyl)prop-2-enoyl>amino)propyl)-N,N'-(butan-1,4-diyl)bis which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

N1-(4-acetoxycinnamoyl)-N4,N8-bis(t-butoxycarbonyl)spermidine (95687-13-1) → Di(tert-butyl)-N-(3-(<(E)-3-(4-hydroxyphenyl)prop-2-enoyl>amino)propyl)-N,N'-(butan-1,4-diyl)bis (69089-01-6)

Guidance literature:

With ammonia; In methanol; at 20 ℃; for 5h;

Reference yield: 88.0%

N1,N5-di-boc-spermidine (68076-39-1) + p-Coumaric Acid (7400-08-0,50940-26-6) → Di(tert-butyl)-N-(3-(<(E)-3-(4-hydroxyphenyl)prop-2-enoyl>amino)propyl)-N,N'-(butan-1,4-diyl)bis (69089-01-6)

Guidance literature:

With dicyclohexyl-carbodiimide; In tetrahydrofuran;

DOI:10.1002/hlca.19960790222

Reference yield:

tert-butyl 2-cyanoethyl-{4-[(tert-butoxycarbonyl)amino]butyl}carbamate (68076-41-5) → Di(tert-butyl)-N-(3-(<(E)-3-(4-hydroxyphenyl)prop-2-enoyl>amino)propyl)-N,N'-(butan-1,4-diyl)bis (69089-01-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 86 percent / H₂, 1 N NaOH / Raney-Ni / ethanol

2: 88 percent / dicyclohexylcarbodiimide / tetrahydrofuran

With sodium hydroxide; hydrogen; dicyclohexyl-carbodiimide; nickel; In tetrahydrofuran; ethanol;

DOI:10.1002/hlca.19960790222

upstream raw materials:

N¹-4-Methansulfonyloxycinnamoyl-N²,N³-di-tert-butoxycarbonyl-spermidin

N¹-(4-acetoxycinnamoyl)-N⁴,N⁸-bis(t-butoxycarbonyl)spermidine

N₁,N₅-di-boc-spermidine

p-Coumaric Acid

Downstream raw materials:

N¹-4-Hydroxy-cinnamoyl-spermidin

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