C₃₇H₅₄N₄O₇

Base Information

Chemical Name:C₃₇H₅₄N₄O₇
CAS No.:1388842-00-9
Molecular Formula:C₃₇H₅₄N₄O₇
Molecular Weight:666.858
Hs Code.:

C<sub>37</sub>H<sub>54</sub>N<sub>4</sub>O<sub>7</sub>

Synonyms:C₃₇H₅₄N₄O₇

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Chemical Property of C₃₇H₅₄N₄O₇

Chemical Property:

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Technology Process of C₃₇H₅₄N₄O₇

There total 8 articles about C₃₇H₅₄N₄O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 124818-94-6,116246-06-1
ethyl (2E,4S)-4-[(tert-butoxycarbonyl)amino]-5-phenylpent-2-enoate

: 1388842-00-9
C₃₇H₅₄N₄O₇

Guidance literature:: Multi-step reaction with 6 steps

1.1: trifluoroacetic acid / dichloromethane / 0.5 h / Cooling with ice

2.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 0.08 h / 0 °C

2.2: 6 h / 0 - 20 °C

3.1: trifluoroacetic acid / dichloromethane / 0.5 h / Cooling with ice

4.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 0.08 h / 0 °C / Cooling

4.2: 4 h / 0 - 20 °C

5.1: palladium on carbon; hydrogen / ethanol / 6 h

6.1: sodium hydroxide / ethanol / 2 h

6.2: pH 3 / Cooling

With palladium on carbon; hydrogen; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; trifluoroacetic acid; sodium hydroxide; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c2cc32911e

Reference yield:

: 72155-45-4
Boc-L-phenylalaninal

: 1388842-00-9
C₃₇H₅₄N₄O₇

Guidance literature:: Multi-step reaction with 7 steps

1.1: tetrahydrofuran / 5 h / 20 °C

2.1: trifluoroacetic acid / dichloromethane / 0.5 h / Cooling with ice

3.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 0.08 h / 0 °C

3.2: 6 h / 0 - 20 °C

4.1: trifluoroacetic acid / dichloromethane / 0.5 h / Cooling with ice

5.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 0.08 h / 0 °C / Cooling

5.2: 4 h / 0 - 20 °C

6.1: palladium on carbon; hydrogen / ethanol / 6 h

7.1: sodium hydroxide / ethanol / 2 h

7.2: pH 3 / Cooling

With palladium on carbon; hydrogen; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; 1.1: Wittig reaction;
DOI:10.1039/c2cc32911e

Reference yield:

: 244033-75-8
(S)-(+)-trans-5-phenyl-4-amino-2-pentenoic acid ethyl ester

: 1388842-00-9
C₃₇H₅₄N₄O₇

Guidance literature:: Multi-step reaction with 5 steps

1.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 0.08 h / 0 °C

1.2: 6 h / 0 - 20 °C

2.1: sodium hydroxide / ethanol / 2 h

2.2: pH 3 / Cooling

3.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 0.08 h / 0 °C / Cooling

3.2: 4 h / 0 - 20 °C

4.1: palladium on carbon; hydrogen / ethanol / 6 h

5.1: sodium hydroxide / ethanol / 2 h

5.2: pH 3 / Cooling

With palladium on carbon; hydrogen; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; sodium hydroxide; In ethanol; N,N-dimethyl-formamide;
DOI:10.1039/c2cc32911e