(Z)-2-((1-(3-chlorophenyl)-3-methyl-5-oxo-4,5-dihydro-1H-pyrazol-4-yl)(p-tolyl)methylene)hydrazinecarbothioamide

Base Information

Chemical Name:(Z)-2-((1-(3-chlorophenyl)-3-methyl-5-oxo-4,5-dihydro-1H-pyrazol-4-yl)(p-tolyl)methylene)hydrazinecarbothioamide
CAS No.:1342898-07-0
Molecular Formula:C₁₉H₁₈ClN₅OS
Molecular Weight:399.904
Hs Code.:

Synonyms:(Z)-2-((1-(3-chlorophenyl)-3-methyl-5-oxo-4,5-dihydro-1H-pyrazol-4-yl)(p-tolyl)methylene)hydrazinecarbothioamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-2-((1-(3-chlorophenyl)-3-methyl-5-oxo-4,5-dihydro-1H-pyrazol-4-yl)(p-tolyl)methylene)hydrazinecarbothioamide

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Technology Process of (Z)-2-((1-(3-chlorophenyl)-3-methyl-5-oxo-4,5-dihydro-1H-pyrazol-4-yl)(p-tolyl)methylene)hydrazinecarbothioamide

There total 1 articles about (Z)-2-((1-(3-chlorophenyl)-3-methyl-5-oxo-4,5-dihydro-1H-pyrazol-4-yl)(p-tolyl)methylene)hydrazinecarbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.33%

: 1203200-73-0
2-(3-chloro-phenyl)-5-methyl-4-(4-methyl-benzoyl)-2,4-dihydro-pyrazol-3-one

: 79-19-6
thiosemicarbazide

: 1342898-07-0
(Z)-2-((1-(3-chlorophenyl)-3-methyl-5-oxo-4,5-dihydro-1H-pyrazol-4-yl)(p-tolyl)methylene)hydrazinecarbothioamide

Guidance literature:: In ethanol; for 6h; Reflux;
DOI:10.1016/j.poly.2013.08.051

Reference yield: 78.88%

: 66-71-7
1,10-Phenanthroline

: copper(II) nitrate trihydrate

: 1342898-07-0
(Z)-2-((1-(3-chlorophenyl)-3-methyl-5-oxo-4,5-dihydro-1H-pyrazol-4-yl)(p-tolyl)methylene)hydrazinecarbothioamide

: Cu((Z)-2-((1-(3-chlorophenyl)-3-methyl-5-oxo-4,5-dihydro-1H-pyrazol-4-yl)(p-tolyl)methylene)hydrazinecarbothioamide)(1,10-phenanthroline)

Guidance literature:: With ammonia; In methanol; for 3h; pH=Ca. 7.5; Reflux;
DOI:10.1016/j.poly.2013.08.051

Reference yield: 66.76%

: 1342898-07-0
(Z)-2-((1-(3-chlorophenyl)-3-methyl-5-oxo-4,5-dihydro-1H-pyrazol-4-yl)(p-tolyl)methylene)hydrazinecarbothioamide

: 142-71-2
copper diacetate

: Cu(2-((1-(3-chlorophenyl)-3-methyl-5-oxo-4,5-dihydro-1H-pyrazol-4-yl)(p-tolyl)methylene)hydrazinecarbothioamide(-2H))(water)

Guidance literature:: With CH₃COONa; In ethanol; water; addn. of aq. soln. of copper compd. to hot ethanolic soln. of hydrozone deriv., addn. of sodium acetate, refluxing for 4 h; filtration, washing with hot water and drying in air, elem. anal.;
DOI:10.1016/j.saa.2011.09.039