C₃₇H₄₄O₈

Base Information

Chemical Name:C₃₇H₄₄O₈
CAS No.:374752-91-7
Molecular Formula:C₃₇H₄₄O₈
Molecular Weight:616.752
Hs Code.:

C<sub>37</sub>H<sub>44</sub>O<sub>8</sub>

Synonyms:C₃₇H₄₄O₈

Suppliers and Price of C₃₇H₄₄O₈

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₇H₄₄O₈

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₇H₄₄O₈

There total 23 articles about C₃₇H₄₄O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 374752-89-3
C₃₇H₄₃IO₈

: 374752-91-7
C₃₇H₄₄O₈

Guidance literature:: With triethyl borane; tri-n-butyl-tin hydride; In hexane; toluene; at -78 ℃; for 1h;
DOI:10.1021/ja016272z

Reference yield:

: 374752-89-3
C₃₇H₄₃IO₈

: 374752-91-7
C₃₇H₄₄O₈

: C₃₇H₄₄O₈

Guidance literature:: With triethyl borane; tri-n-butyl-tin hydride; In hexane; toluene; at -78 ℃; for 1h; Title compound not separated from byproducts.;
DOI:10.1021/ja0279646

Reference yield:

: 482626-35-7
(2R,3S,4S,5S)-5-Benzyloxymethoxy-7-(4-methoxy-benzyloxy)-2,4-dimethyl-heptane-1,3-diol

: 374752-91-7
C₃₇H₄₄O₈

Guidance literature:: Multi-step reaction with 15 steps

1: 100 percent / imidazole / CH₂Cl₂ / 1 h / 0 °C

2: 93 percent / NaHMDS / tetrahydrofuran; dimethylformamide / 1 h / 20 °C

3: 93 percent / tetrabutylammonium fluoride / tetrahydrofuran / 8 h / 20 °C

4: 96 percent / triethylamine; sulfur trioxide pyridine complex / dimethylsulfoxide; CH₂Cl₂ / 3 h / 20 °C

5: 99 percent / MgBr₂*Et₂O / CH₂Cl₂ / 3 h / 20 °C

6: osmium tetroxide; NMO / acetone; H₂O / 1.5 h / 20 °C

7: NaIO₄ / acetone; H₂O / 0.5 h / 20 °C

8: 3.24 g / NaBH₄ / ethanol / 0.5 h / 20 °C

9: 93 percent / pyridine; DMAP / CH₂Cl₂ / 24 h / 20 °C

10: 88 percent / CAN / acetonitrile; H₂O / 0.5 h / 20 °C

11: 99 percent / triethylamine / CH₂Cl₂ / 3 h / 0 °C

12: 99 percent / aq. HCl / acetonitrile / 2 h / 20 °C

13: 68 percent / p-TsOH*H₂O / CHCl₃ / 12 h / Heating

14: 99 percent / NaI / acetone / 2 h / Heating

15: Bu₃SnH; Et₃B / toluene; hexane / 1 h / -78 °C

With pyridine; 1H-imidazole; hydrogenchloride; dmap; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; N-methyl-2-indolinone; ammonium cerium(IV) nitrate; triethyl borane; tetrabutyl ammonium fluoride; tri-n-butyl-tin hydride; sodium hexamethyldisilazane; sulfur trioxide pyridine complex; toluene-4-sulfonic acid; triethylamine; sodium iodide; magnesium bromide; In tetrahydrofuran; ethanol; hexane; dichloromethane; chloroform; water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetone; toluene; acetonitrile;
DOI:10.1021/ja0279646