diazomethane

Base Information

• Chemical Name: diazomethane
• CAS No.: 136391-65-6
• Molecular Formula: C₁₀H₁₀N₂O₂
• Molecular Weight: 190.202

Synonyms:diazomethane

Chemical Property of diazomethane

Chemical Property:

Purity/Quality:

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Technology Process of diazomethane

There total 3 articles about diazomethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ diazomethane (136391-65-6)

Guidance literature:

With sodium hydroxide;

Reference yield:

ethyl 2-formylbenzoate (34046-43-0) + toluene-4-sulfonic acid hydrazide (1576-35-8) → diazomethane (136391-65-6)

Guidance literature:

With sodium hydride; Yield given. Multistep reaction; 1.) THF, RT, 2.) 140 deg C, 2-5 * 10^-5 Torr, 30 min;

Reference yield:

2,3-Dihydro-2-nitroso-1H-isoindol-1-on (5415-18-9) → diazomethane (136391-65-6)

Guidance literature:

upstream raw materials:

ethyl 2-formylbenzoate

toluene-4-sulfonic acid hydrazide

2,3-Dihydro-2-nitroso-1H-isoindol-1-on

Downstream raw materials:

ethyl 2-(ethoxymethyl)benzoate

2-benzofuran-1(3H)-one

3-ethylphthalide

2-ethoxy-1(2H)-benzocyclobutenone

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