Technology Process of C11H20O4
There total 4 articles about C11H20O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: lithium hexamethyldisilazane / tetrahydrofuran / 2 h / -78 - 20 °C
2: potassium hydrogencarbonate / tetrahydrofuran; water / 2 h / -78 °C
3: 1H-imidazole / dichloromethane / 3 h
4: sodium tetrahydroborate; cerium(III) chloride heptahydrate / methanol / 0.25 h
5: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h
With
1H-imidazole; sodium tetrahydroborate; cerium(III) chloride heptahydrate; tetrabutyl ammonium fluoride; potassium hydrogencarbonate; lithium hexamethyldisilazane;
In
tetrahydrofuran; methanol; dichloromethane; water;
4: Luche reduction;
DOI:10.1016/j.tetlet.2011.12.015
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1H-imidazole / dichloromethane / 3 h
2: sodium tetrahydroborate; cerium(III) chloride heptahydrate / methanol / 0.25 h
3: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h
With
1H-imidazole; sodium tetrahydroborate; cerium(III) chloride heptahydrate; tetrabutyl ammonium fluoride;
In
tetrahydrofuran; methanol; dichloromethane;
2: Luche reduction;
DOI:10.1016/j.tetlet.2011.12.015