(eta.5-C₅Me₅)2ScCH₃

Base Information

Chemical Name:(eta.5-C₅Me₅)2ScCH₃
CAS No.:99707-15-0
Molecular Formula:C₂₁H₃₃Sc
Molecular Weight:330.449
Hs Code.:

(eta.5-C<sub>5</sub>Me<sub>5</sub>)2ScCH<sub>3</sub>

Synonyms:(eta.5-C₅Me₅)2ScCH₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (eta.5-C₅Me₅)2ScCH₃

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Technology Process of (eta.5-C₅Me₅)2ScCH₃

There total 1 articles about (eta.5-C₅Me₅)2ScCH₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 34557-54-5,27936-85-2
methane

: 586367-34-2
[(η5-pentamethylcyclopentadienide)Sc(CH2C(CH3)3]

: 99707-15-0
(eta.5-C₅Me₅)2ScCH₃

: 463-82-1
2,2-dimethylpropane

Guidance literature:: In Cyclohexane-d12; under Ar, in the dark; in NMR tube; CH4 added to soln. of Sc complex in cyclohexane-d12 at 77 K; warmed to 11-50°C; not isolated; monitored by (1)H NMR spectra; Kinetics;
DOI:10.1021/ja021341a

Reference yield: 67.0%

: 99707-15-0
(eta.5-C₅Me₅)2ScCH₃

: N,N-dimethylanilinium tetraphenylborate

: 869648-30-6
decamethylscandocene*BPh₄

Guidance literature:: In toluene; byproducts: CH4, (C6H5)N(CH3)2; (Schlenk; N2 atm.) toluene was added to a mixt. of complexes, 1 h; the solvent was evapd., the solid was washed with pentane; elem. anal.;
DOI:10.1021/ja054544i

Reference yield: 65.0%

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: 99707-15-0
(eta.5-C₅Me₅)2ScCH₃

: N,N-dimethylanilinium tetraphenylborate

: 869648-74-8
[(η5-C5Me5)2Sc(THF)2][BPh4]

Guidance literature:: In tetrahydrofuran; (Schlenk; N2 atm.) THF was added to a mixt. of complexes; pentane was carefully layered on top of the mixt.; elem. anal.;
DOI:10.1021/ja054544i