C₃₁H₅₂O₅SSi

Base Information

Chemical Name:C₃₁H₅₂O₅SSi
CAS No.:934618-00-5
Molecular Formula:C₃₁H₅₂O₅SSi
Molecular Weight:564.902
Hs Code.:

C<sub>31</sub>H<sub>52</sub>O<sub>5</sub>SSi

Synonyms:C₃₁H₅₂O₅SSi

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Chemical Property of C₃₁H₅₂O₅SSi

Chemical Property:

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Technology Process of C₃₁H₅₂O₅SSi

There total 10 articles about C₃₁H₅₂O₅SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 934617-99-9
C₃₂H₅₆O₈S₂Si

: 934618-00-5
C₃₁H₅₂O₅SSi

Guidance literature:: With potassium carbonate; In methanol; dichloromethane;
DOI:10.1246/cl.2007.278

Reference yield:

: C₁₃H₁₆O₃

: 934618-00-5
C₃₁H₅₂O₅SSi

Guidance literature:: Multi-step reaction with 8 steps

1.1: H₂ / Pd/C / ethyl acetate

2.1: 71 percent / Mg; HgCl₂ / diethyl ether / -50 - -15 °C

3.1: 100 percent / 2,6-lutidine / CH₂Cl₂

4.1: ZnI₂; n-Bu₄NI / 1,2-dichloro-ethane

4.2: Ac₂O; AcOH / dimethylsulfoxide / 70 °C

5.1: 92 percent / n-BuLi; BF₃*OEt₂ / tetrahydrofuran / -78 °C

6.1: 100 percent / TEA; DMAP / CH₂Cl₂

7.1: 94 percent / AcOH; H₂O / tetrahydrofuran / 50 °C

8.1: 98 percent / K₂CO₃ / methanol; CH₂Cl₂

With 2,6-dimethylpyridine; dmap; n-butyllithium; TEA; boron trifluoride diethyl etherate; water; hydrogen; tetra-(n-butyl)ammonium iodide; potassium carbonate; magnesium; acetic acid; mercury dichloride; zinc(II) iodide; palladium on activated charcoal; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; ethyl acetate; 1,2-dichloro-ethane;
DOI:10.1246/cl.2007.278

Reference yield:

: 102490-00-6
(2S,3R)-1,2-epoxy-4-penten-3-ol

: 934618-00-5
C₃₁H₅₂O₅SSi

Guidance literature:: Multi-step reaction with 9 steps

1.1: i-Pr₂NEt; n-Bu₄NI / 1,2-dichloro-ethane / 50 °C

2.1: H₂ / Pd/C / ethyl acetate

3.1: 71 percent / Mg; HgCl₂ / diethyl ether / -50 - -15 °C

4.1: 100 percent / 2,6-lutidine / CH₂Cl₂

5.1: ZnI₂; n-Bu₄NI / 1,2-dichloro-ethane

5.2: Ac₂O; AcOH / dimethylsulfoxide / 70 °C

6.1: 92 percent / n-BuLi; BF₃*OEt₂ / tetrahydrofuran / -78 °C

7.1: 100 percent / TEA; DMAP / CH₂Cl₂

8.1: 94 percent / AcOH; H₂O / tetrahydrofuran / 50 °C

9.1: 98 percent / K₂CO₃ / methanol; CH₂Cl₂

With 2,6-dimethylpyridine; dmap; n-butyllithium; TEA; boron trifluoride diethyl etherate; water; hydrogen; tetra-(n-butyl)ammonium iodide; potassium carbonate; magnesium; acetic acid; N-ethyl-N,N-diisopropylamine; mercury dichloride; zinc(II) iodide; palladium on activated charcoal; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; ethyl acetate; 1,2-dichloro-ethane;
DOI:10.1246/cl.2007.278