sodium (2-chloro-6-phenyl-pyridin-3-yl)-methoxymethyl trifluoroborate

Base Information

Chemical Name:sodium (2-chloro-6-phenyl-pyridin-3-yl)-methoxymethyl trifluoroborate
CAS No.:1013915-70-2
Molecular Formula:C₁₃H₁₁BClF₃NO*Na
Molecular Weight:323.485
Hs Code.:

Synonyms:sodium (2-chloro-6-phenyl-pyridin-3-yl)-methoxymethyl trifluoroborate

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Chemical Property of sodium (2-chloro-6-phenyl-pyridin-3-yl)-methoxymethyl trifluoroborate

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Technology Process of sodium (2-chloro-6-phenyl-pyridin-3-yl)-methoxymethyl trifluoroborate

There total 1 articles about sodium (2-chloro-6-phenyl-pyridin-3-yl)-methoxymethyl trifluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.0%

: 275383-94-3
2-chloro-3-(hydroxymethyl)-6-phenylpyridine

: 70557-99-2
2-(iodomethyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1013915-70-2
sodium (2-chloro-6-phenyl-pyridin-3-yl)-methoxymethyl trifluoroborate

Guidance literature:: 2-chloro-3-(hydroxymethyl)-6-phenylpyridine; With sodium hydride; In tetrahydrofuran; at 0 - 20 ℃; for 1h;

2-(iodomethyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane; In tetrahydrofuran; at 0 - 20 ℃; for 14h;

With sodium difluorohydrogenate; water; more than 3 stages;

Reference yield: 5.0%

: 1013915-70-2
sodium (2-chloro-6-phenyl-pyridin-3-yl)-methoxymethyl trifluoroborate

: 1013915-49-5
2-phenyl-5,7-dihydro-furo[3,4-b]pyridine

Guidance literature:: With caesium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; water; at 20 - 140 ℃; for 0.25h; Microwave irradiation;