Technology Process of C28H36N6O8
There total 11 articles about C28H36N6O8 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C34H46N6O10;
With
lithium hydroxide monohydrate;
In
tetrahydrofuran; methanol; water;
at 20 ℃;
for 18h;
With
acetic acid;
In
tetrahydrofuran; methanol; water;
DOI:10.1016/j.tet.2012.09.002
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: ammonium acetate; acetic acid / methanol / 64 h / 60 °C
2.1: N,N-dimethyl-formamide / -10 - 20 °C
3.1: palladium on activated charcoal; hydrogen / ethanol / 50 °C / 750.08 Torr
4.1: 2,4,6-trimethyl-pyridine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 0.25 h / 20 °C
4.2: 2 h
5.1: lithium hydroxide monohydrate / tetrahydrofuran; methanol; water / 18 h / 20 °C
With
2,4,6-trimethyl-pyridine; lithium hydroxide monohydrate; palladium on activated charcoal; ammonium acetate; hydrogen; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; acetic acid;
In
tetrahydrofuran; methanol; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2012.09.002
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: N,N-dimethyl-formamide / -10 - 20 °C
2.1: palladium on activated charcoal; hydrogen / ethanol / 50 °C / 750.08 Torr
3.1: 2,4,6-trimethyl-pyridine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 0.25 h / 20 °C
3.2: 2 h
4.1: lithium hydroxide monohydrate / tetrahydrofuran; methanol; water / 18 h / 20 °C
With
2,4,6-trimethyl-pyridine; lithium hydroxide monohydrate; palladium on activated charcoal; hydrogen; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate;
In
tetrahydrofuran; methanol; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2012.09.002
