5-(2,2-dimethyl-1,3-dioxolan-4-yl)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-6-ol

Base Information

• Chemical Name: 5-(2,2-dimethyl-1,3-dioxolan-4-yl)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-6-ol
• CAS No.: 207855-12-7
• Molecular Formula: C₁₂H₂₀O₆
• Molecular Weight: 260.287
• Mol file: 207855-12-7.mol

Synonyms:5-(2,2-Dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-ol

Chemical Property of 5-(2,2-dimethyl-1,3-dioxolan-4-yl)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-6-ol

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 5-(2,2-dimethyl-1,3-dioxolan-4-yl)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-6-ol

There total 3 articles about 5-(2,2-dimethyl-1,3-dioxolan-4-yl)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-6-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

Carbonic acid allyl ester 5-(2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl ester → 5-(2,2-Dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-ol (207855-12-7)

Guidance literature:

With diethylamine; palladium diacetate; trisodium tris(3-sulfophenyl)phosphine; In water; acetonitrile; for 0.166667h; Ambient temperature;

DOI:10.1016/S0040-4020(01)80771-7

Reference yield: 95.0%

6-allyloxy-5-(2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxole → 5-(2,2-Dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-ol (207855-12-7)

Guidance literature:

With chloro-trimethyl-silane; sodium cyanoborohydride; In acetonitrile; at 20 ℃; for 0.25h;

DOI:10.1080/00397910008087271

Reference yield: 75.0%

5-(2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-6-(tetrahydro-pyran-2-yloxy)-tetrahydro-furo[2,3-d][1,3]dioxole → 5-(2,2-Dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-ol (207855-12-7)

Guidance literature:

With water; β‐cyclodextrin; In methanol; at 50 ℃; for 12h;

DOI:10.1039/b009187l