(S)-2-(dibenzylamino)-3-phenyl-1-bromopropane

Base Information

Chemical Name:(S)-2-(dibenzylamino)-3-phenyl-1-bromopropane
CAS No.:208103-10-0
Molecular Formula:C₂₃H₂₄BrN
Molecular Weight:394.354
Hs Code.:

Synonyms:(S)-2-(dibenzylamino)-3-phenyl-1-bromopropane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-2-(dibenzylamino)-3-phenyl-1-bromopropane

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Technology Process of (S)-2-(dibenzylamino)-3-phenyl-1-bromopropane

There total 3 articles about (S)-2-(dibenzylamino)-3-phenyl-1-bromopropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 111060-52-7
(S)-2-(dibenzylamino)-3-phenylpropan-1-ol

: 208103-10-0
(S)-2-(dibenzylamino)-3-phenyl-1-bromopropane

Guidance literature:: With sulfurous dibromide; In tetrahydrofuran; at 50 ℃; for 3h;
DOI:10.1002/hlca.19980810506

Reference yield:

: 63-91-2,25191-15-5,658-69-5,67675-33-6
L-phenylalanine

: 208103-10-0
(S)-2-(dibenzylamino)-3-phenyl-1-bromopropane

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / NaOH, K₂CO₃ / H₂O; ethanol / 1.5 h / Heating

2: 82 percent / LiAlH₄ / diethyl ether / Ambient temperature

3: 75 percent / SOBr₂ / tetrahydrofuran / 3 h / 50 °C

With sodium hydroxide; lithium aluminium tetrahydride; sulfurous dibromide; potassium carbonate; In tetrahydrofuran; diethyl ether; ethanol; water;
DOI:10.1002/hlca.19980810506

Reference yield:

: 111138-83-1
N,N-dibenzyl-L-phenylalanine benzyl ester

: 208103-10-0
(S)-2-(dibenzylamino)-3-phenyl-1-bromopropane

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / LiAlH₄ / diethyl ether / Ambient temperature

2: 75 percent / SOBr₂ / tetrahydrofuran / 3 h / 50 °C

With lithium aluminium tetrahydride; sulfurous dibromide; In tetrahydrofuran; diethyl ether;
DOI:10.1002/hlca.19980810506