C₁₄H₁₈O

Base Information

• Chemical Name: C₁₄H₁₈O
• CAS No.: 1209385-97-6
• Molecular Formula: C₁₄H₁₈O
• Molecular Weight: 202.296

Synonyms:C₁₄H₁₈O

Chemical Property of C₁₄H₁₈O

Chemical Property:

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Technology Process of C₁₄H₁₈O

There total 1 articles about C₁₄H₁₈O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

O-benzyl 2,2,2-trichloroacetimidate (81927-55-1) + (S)-Hept-5-yn-3-ol → C14H18O (1209385-97-6)

Guidance literature:

With trifluorormethanesulfonic acid; In dichloromethane; cyclohexane; at 20 ℃; for 6h; Inert atmosphere;

DOI:10.1021/jo400260m

Reference yield: 77.0%

C14H18O (1209385-97-6) → C14H19IO

Guidance literature:

C₁₄H₁₈O; With zirconocene dichloride; diisobutylaluminium hydride; In tetrahydrofuran; hexane; at 0 - 50 ℃; Inert atmosphere; Darkness;

With N-iodo-succinimide; In tetrahydrofuran; at 0 ℃; for 0.166667h; regioselective reaction; Inert atmosphere;

DOI:10.1021/jo400260m

Reference yield:

C14H18O (1209385-97-6) → C18H24O3

Guidance literature:

Multi-step reaction with 2 steps

1.1: diisobutylaluminium hydride; zirconocene dichloride / tetrahydrofuran; hexane / 0 - 50 °C / Inert atmosphere; Darkness

1.2: 0.17 h / 0 °C / Inert atmosphere

2.1: palladium diacetate; sodium hydrogencarbonate; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 8 h / 100 °C / Inert atmosphere; Sealed tube

With zirconocene dichloride; palladium diacetate; tetra-(n-butyl)ammonium iodide; diisobutylaluminium hydride; sodium hydrogencarbonate; In tetrahydrofuran; hexane; N,N-dimethyl-formamide; 2.1: |Heck Reaction;

DOI:10.1021/jo400260m

upstream raw materials:

O-benzyl 2,2,2-trichloroacetimidate

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