15-{[4-(trityl-amino)-butyl]-[3-(trityl-amino)-propyl]-carbamoyl}-pentadecanoic acid 2-oxo-2-phenyl-ethyl ester

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Chemical Name:15-{[4-(trityl-amino)-butyl]-[3-(trityl-amino)-propyl]-carbamoyl}-pentadecanoic acid 2-oxo-2-phenyl-ethyl ester
CAS No.:443770-21-6
Molecular Formula:C₆₉H₈₁N₃O₄
Molecular Weight:1016.42
Hs Code.:

Synonyms:15-{[4-(trityl-amino)-butyl]-[3-(trityl-amino)-propyl]-carbamoyl}-pentadecanoic acid 2-oxo-2-phenyl-ethyl ester

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Chemical Property of 15-{[4-(trityl-amino)-butyl]-[3-(trityl-amino)-propyl]-carbamoyl}-pentadecanoic acid 2-oxo-2-phenyl-ethyl ester

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Technology Process of 15-{[4-(trityl-amino)-butyl]-[3-(trityl-amino)-propyl]-carbamoyl}-pentadecanoic acid 2-oxo-2-phenyl-ethyl ester

There total 6 articles about 15-{[4-(trityl-amino)-butyl]-[3-(trityl-amino)-propyl]-carbamoyl}-pentadecanoic acid 2-oxo-2-phenyl-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 244033-13-4
N^α,N^ω-ditritylspermidine

: 443770-14-7
hexadecanedioic acid mono-(2-oxo-2-phenyl-ethyl) ester

: 443770-21-6
15-{[4-(trityl-amino)-butyl]-[3-(trityl-amino)-propyl]-carbamoyl}-pentadecanoic acid 2-oxo-2-phenyl-ethyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; In N,N-dimethyl-formamide; at 0 - 25 ℃; for 24.5h;
DOI:10.1016/S0040-4039(02)00338-6

Reference yield:

: 505-54-4
thapsic acid

: 443770-21-6
15-{[4-(trityl-amino)-butyl]-[3-(trityl-amino)-propyl]-carbamoyl}-pentadecanoic acid 2-oxo-2-phenyl-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / iPr₂NEt / dimethylformamide / 24 h / 25 °C

2: 70 percent / bromotripyrrolidinophosphonium hexafluorophosphate; iPr₂NEt / dimethylformamide / 24.5 h / 0 - 25 °C

With N-ethyl-N,N-diisopropylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(02)00338-6

Reference yield:

: 189341-61-5
N₁-Triphenylmethyl-1,4-diaminobutane

: 443770-21-6
15-{[4-(trityl-amino)-butyl]-[3-(trityl-amino)-propyl]-carbamoyl}-pentadecanoic acid 2-oxo-2-phenyl-ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N / dimethylformamide / 1.5 h / 0 - 25 °C

2: 65 percent / LiAlH₄ / tetrahydrofuran / 48 h / Heating

3: 70 percent / bromotripyrrolidinophosphonium hexafluorophosphate; iPr₂NEt / dimethylformamide / 24.5 h / 0 - 25 °C

With lithium aluminium tetrahydride; triethylamine; N-ethyl-N,N-diisopropylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(02)00338-6