N₁-(2-(diethylamino)ethyl)-N₄-((S)-1-((S,E)-5-methyl-1-(methylsulfonyl)hex-1-en-3-ylamino)-1-oxo-3-phenylpropan-2-yl)terephthalamide

Base Information

• Chemical Name: N₁-(2-(diethylamino)ethyl)-N₄-((S)-1-((S,E)-5-methyl-1-(methylsulfonyl)hex-1-en-3-ylamino)-1-oxo-3-phenylpropan-2-yl)terephthalamide
• CAS No.: 1346804-64-5
• Molecular Formula: C₃₁H₄₄N₄O₅S
• Molecular Weight: 584.78

Synonyms:N₁-(2-(diethylamino)ethyl)-N₄-((S)-1-((S,E)-5-methyl-1-(methylsulfonyl)hex-1-en-3-ylamino)-1-oxo-3-phenylpropan-2-yl)terephthalamide

Chemical Property of N₁-(2-(diethylamino)ethyl)-N₄-((S)-1-((S,E)-5-methyl-1-(methylsulfonyl)hex-1-en-3-ylamino)-1-oxo-3-phenylpropan-2-yl)terephthalamide

Chemical Property:

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Technology Process of N₁-(2-(diethylamino)ethyl)-N₄-((S)-1-((S,E)-5-methyl-1-(methylsulfonyl)hex-1-en-3-ylamino)-1-oxo-3-phenylpropan-2-yl)terephthalamide

There total 1 articles about N₁-(2-(diethylamino)ethyl)-N₄-((S)-1-((S,E)-5-methyl-1-(methylsulfonyl)hex-1-en-3-ylamino)-1-oxo-3-phenylpropan-2-yl)terephthalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

N-(2-diethylamino-ethyl)-N'-[1-(1-formyl-3-methyl-butylcarbamoyl)-2-phenyl-ethyl]-terephthalamide + diethyl methylsulfonylmethylphosphonate (40137-11-9) → N1-(2-(diethylamino)ethyl)-N4-((S)-1-((S,E)-5-methyl-1-(methylsulfonyl)hex-1-en-3-ylamino)-1-oxo-3-phenylpropan-2-yl)terephthalamide (1346804-64-5)

Guidance literature:

diethyl methylsulfonylmethylphosphonate; With sodium hydride; In tetrahydrofuran; mineral oil; at -70 ℃; for 0.5h; Inert atmosphere;

N-(2-diethylamino-ethyl)-N'-[1-(1-formyl-3-methyl-butylcarbamoyl)-2-phenyl-ethyl]-terephthalamide; In tetrahydrofuran; mineral oil; at -70 ℃; Inert atmosphere;

DOI:10.1016/j.ejmech.2011.07.037

upstream raw materials:

diethyl methylsulfonylmethylphosphonate

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