[[8-acetyl-7-[5-(4-acetyl-3-hydroxy-2-propylphenoxy)pentyloxy]-2-naphthalenyl]oxy]acetic acid

Base Information

Chemical Name:[[8-acetyl-7-[5-(4-acetyl-3-hydroxy-2-propylphenoxy)pentyloxy]-2-naphthalenyl]oxy]acetic acid
CAS No.:101463-98-3
Molecular Formula:C₃₀H₃₄O₈
Molecular Weight:522.595
Hs Code.:

Synonyms:[[8-acetyl-7-[5-(4-acetyl-3-hydroxy-2-propylphenoxy)pentyloxy]-2-naphthalenyl]oxy]acetic acid

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Chemical Property of [[8-acetyl-7-[5-(4-acetyl-3-hydroxy-2-propylphenoxy)pentyloxy]-2-naphthalenyl]oxy]acetic acid

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Technology Process of [[8-acetyl-7-[5-(4-acetyl-3-hydroxy-2-propylphenoxy)pentyloxy]-2-naphthalenyl]oxy]acetic acid

There total 6 articles about [[8-acetyl-7-[5-(4-acetyl-3-hydroxy-2-propylphenoxy)pentyloxy]-2-naphthalenyl]oxy]acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 101463-97-2
[[8-Acetyl-7-[5-(4-acetyl-3-hydroxy-2-propylphenoxy)-pentyloxy]-2-naphthalenyl]oxy]acetic acid methyl ester

: 101463-98-3
[[8-acetyl-7-[5-(4-acetyl-3-hydroxy-2-propylphenoxy)pentyloxy]-2-naphthalenyl]oxy]acetic acid

Guidance literature:: With sodium hydroxide; In methanol; for 5h; Heating;
DOI:10.1021/jm00384a029

Reference yield:

: 111-24-0
1,5-dibromo-pentane

: 101463-98-3
[[8-acetyl-7-[5-(4-acetyl-3-hydroxy-2-propylphenoxy)pentyloxy]-2-naphthalenyl]oxy]acetic acid

Guidance literature:: Multi-step reaction with 3 steps

1: K₂CO₃ / acetone / 17 h / Heating

2: 69 percent / K₂CO₃ / acetone / 20 h / Heating

3: 78 percent / 1N NaOH / methanol / 5 h / Heating

With sodium hydroxide; potassium carbonate; In methanol; acetone;
DOI:10.1021/jm00384a029

Reference yield:

: 582-17-2
2,7-Dihydroxynaphthalene

: 101463-98-3
[[8-acetyl-7-[5-(4-acetyl-3-hydroxy-2-propylphenoxy)pentyloxy]-2-naphthalenyl]oxy]acetic acid

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) K₂CO₃ / 1.) acetone, 22 deg C, 3 h, 2.) acetone, 22 deg C, 19 h

2: 63 percent / AlCl₃ / 1,2-dichloro-ethane / a) 22 deg C, 2 h, b) reflux, 19 h

3: K₂CO₃ / acetone / 17 h / Heating

4: 69 percent / K₂CO₃ / acetone / 20 h / Heating

5: 78 percent / 1N NaOH / methanol / 5 h / Heating

With sodium hydroxide; aluminium trichloride; potassium carbonate; In methanol; 1,2-dichloro-ethane; acetone;
DOI:10.1021/jm00384a029