methyl 6-O-acetyl-2,3-di-O-benzoyl-4-(2-((naphthalen-2-ylmethoxy)methyl)benzoyl)-α-D-glucopyranoside

Base Information

Chemical Name:methyl 6-O-acetyl-2,3-di-O-benzoyl-4-(2-((naphthalen-2-ylmethoxy)methyl)benzoyl)-α-D-glucopyranoside
CAS No.:1504584-89-7
Molecular Formula:C₄₂H₃₈O₁₁
Molecular Weight:718.757
Hs Code.:

Synonyms:methyl 6-O-acetyl-2,3-di-O-benzoyl-4-(2-((naphthalen-2-ylmethoxy)methyl)benzoyl)-α-D-glucopyranoside

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Chemical Property of methyl 6-O-acetyl-2,3-di-O-benzoyl-4-(2-((naphthalen-2-ylmethoxy)methyl)benzoyl)-α-D-glucopyranoside

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Technology Process of methyl 6-O-acetyl-2,3-di-O-benzoyl-4-(2-((naphthalen-2-ylmethoxy)methyl)benzoyl)-α-D-glucopyranoside

There total 4 articles about methyl 6-O-acetyl-2,3-di-O-benzoyl-4-(2-((naphthalen-2-ylmethoxy)methyl)benzoyl)-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1504584-76-2
2-((naphthalen-2-ylmethoxy)methyl)benzoic acid

: methyl 6-O-acetyl-2,3-di-O-benzoyl-α-D-glucopyranoside

: 1504584-89-7
methyl 6-O-acetyl-2,3-di-O-benzoyl-4-(2-((naphthalen-2-ylmethoxy)methyl)benzoyl)-α-D-glucopyranoside

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1039/c3cc49205b

Reference yield:

: 4137-35-3,23397-67-3,102518-21-8,109681-62-1,117124-69-3,149035-49-4
methyl 2,3-di-O-benzoyl-α-D-glucopyranoside

: 1504584-89-7
methyl 6-O-acetyl-2,3-di-O-benzoyl-4-(2-((naphthalen-2-ylmethoxy)methyl)benzoyl)-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 2,4,6-trimethyl-pyridine / 19 h / -40 - 20 °C / Inert atmosphere

2: dicyclohexyl-carbodiimide; dmap / dichloromethane / 3 h / 20 °C / Inert atmosphere

With 2,4,6-trimethyl-pyridine; dmap; dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1039/c3cc49205b

Reference yield:

: 939-26-4
2-bromomethylnaphthyl bromide

: 1504584-89-7
methyl 6-O-acetyl-2,3-di-O-benzoyl-4-(2-((naphthalen-2-ylmethoxy)methyl)benzoyl)-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide / toluene / 48 h / Reflux; Inert atmosphere

2: dicyclohexyl-carbodiimide; dmap / dichloromethane / 3 h / 20 °C / Inert atmosphere

With dmap; dicyclohexyl-carbodiimide; potassium hydroxide; In dichloromethane; toluene;
DOI:10.1039/c3cc49205b