2-((E)-2-{4-[(E)-2-(3,4,5-Tris-dodecyloxy-phenyl)-vinyl]-phenyl}-vinyl)-6,7,9,10,12,13,15,16,18,19-decahydro-5,8,11,14,17,20-hexaoxa-benzocyclooctadecene

Base Information

Chemical Name:2-((E)-2-{4-[(E)-2-(3,4,5-Tris-dodecyloxy-phenyl)-vinyl]-phenyl}-vinyl)-6,7,9,10,12,13,15,16,18,19-decahydro-5,8,11,14,17,20-hexaoxa-benzocyclooctadecene
CAS No.:527736-38-5
Molecular Formula:C₆₈H₁₀₈O₉
Molecular Weight:1069.6
Hs Code.:

Synonyms:2-((E)-2-{4-[(E)-2-(3,4,5-Tris-dodecyloxy-phenyl)-vinyl]-phenyl}-vinyl)-6,7,9,10,12,13,15,16,18,19-decahydro-5,8,11,14,17,20-hexaoxa-benzocyclooctadecene

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Chemical Property of 2-((E)-2-{4-[(E)-2-(3,4,5-Tris-dodecyloxy-phenyl)-vinyl]-phenyl}-vinyl)-6,7,9,10,12,13,15,16,18,19-decahydro-5,8,11,14,17,20-hexaoxa-benzocyclooctadecene

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Technology Process of 2-((E)-2-{4-[(E)-2-(3,4,5-Tris-dodecyloxy-phenyl)-vinyl]-phenyl}-vinyl)-6,7,9,10,12,13,15,16,18,19-decahydro-5,8,11,14,17,20-hexaoxa-benzocyclooctadecene

There total 5 articles about 2-((E)-2-{4-[(E)-2-(3,4,5-Tris-dodecyloxy-phenyl)-vinyl]-phenyl}-vinyl)-6,7,9,10,12,13,15,16,18,19-decahydro-5,8,11,14,17,20-hexaoxa-benzocyclooctadecene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 60835-74-7
4'-formyl-benzo-18-crown-6-ether

: 527736-37-4
{4-[(E)-2-(3,4,5-Tris-dodecyloxy-phenyl)-vinyl]-benzyl}-phosphonic acid diethyl ester

: 527736-38-5
2-((E)-2-{4-[(E)-2-(3,4,5-Tris-dodecyloxy-phenyl)-vinyl]-phenyl}-vinyl)-6,7,9,10,12,13,15,16,18,19-decahydro-5,8,11,14,17,20-hexaoxa-benzocyclooctadecene

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1016/S0040-4039(03)00560-4

Reference yield:

: 253598-62-8
(E)-4-[2-(3,4,5-tridodecyloxyphenyl)ethenyl]benzaldehyde

: 527736-38-5
2-((E)-2-{4-[(E)-2-(3,4,5-Tris-dodecyloxy-phenyl)-vinyl]-phenyl}-vinyl)-6,7,9,10,12,13,15,16,18,19-decahydro-5,8,11,14,17,20-hexaoxa-benzocyclooctadecene

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / LiAlH₄ / tetrahydrofuran / 0 °C

2: TMSBr / CHCl₃ / 0 °C

3: 150 °C

4: 82 percent / t-BuOK / tetrahydrofuran / 0 - 20 °C

With lithium aluminium tetrahydride; trimethylsilyl bromide; potassium tert-butylate; In tetrahydrofuran; chloroform; 3: Arbuzov reaction;
DOI:10.1016/S0040-4039(03)00560-4

Reference yield:

: 527736-36-3
5-[(E)-2-(4-Bromomethyl-phenyl)-vinyl]-1,2,3-tris-dodecyloxy-benzene

: 527736-38-5
2-((E)-2-{4-[(E)-2-(3,4,5-Tris-dodecyloxy-phenyl)-vinyl]-phenyl}-vinyl)-6,7,9,10,12,13,15,16,18,19-decahydro-5,8,11,14,17,20-hexaoxa-benzocyclooctadecene

Guidance literature:: Multi-step reaction with 2 steps

1: 150 °C

2: 82 percent / t-BuOK / tetrahydrofuran / 0 - 20 °C

With potassium tert-butylate; In tetrahydrofuran; 1: Arbuzov reaction;
DOI:10.1016/S0040-4039(03)00560-4