(4S,5S)-2-((4S,5S)-1,3-bis(3,5-di-tert-butylbenzyl)-4,5-diphenylimidazolidin-2-ylideneamino)-1,3-dimethyl-4,5-diphenyl-4,5-dihydro-1H-imidazol-3-ium chloride

Base Information

Chemical Name:(4S,5S)-2-((4S,5S)-1,3-bis(3,5-di-tert-butylbenzyl)-4,5-diphenylimidazolidin-2-ylideneamino)-1,3-dimethyl-4,5-diphenyl-4,5-dihydro-1H-imidazol-3-ium chloride
CAS No.:1397644-13-1
Molecular Formula:C₆₂H₇₆N₅*Cl
Molecular Weight:926.772
Hs Code.:

(4S,5S)-2-((4S,5S)-1,3-bis(3,5-di-tert-butylbenzyl)-4,5-diphenylimidazolidin-2-ylideneamino)-1,3-dimethyl-4,5-diphenyl-4,5-dihydro-1H-imidazol-3-ium chloride

Synonyms:(4S,5S)-2-((4S,5S)-1,3-bis(3,5-di-tert-butylbenzyl)-4,5-diphenylimidazolidin-2-ylideneamino)-1,3-dimethyl-4,5-diphenyl-4,5-dihydro-1H-imidazol-3-ium chloride

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Chemical Property of (4S,5S)-2-((4S,5S)-1,3-bis(3,5-di-tert-butylbenzyl)-4,5-diphenylimidazolidin-2-ylideneamino)-1,3-dimethyl-4,5-diphenyl-4,5-dihydro-1H-imidazol-3-ium chloride

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Technology Process of (4S,5S)-2-((4S,5S)-1,3-bis(3,5-di-tert-butylbenzyl)-4,5-diphenylimidazolidin-2-ylideneamino)-1,3-dimethyl-4,5-diphenyl-4,5-dihydro-1H-imidazol-3-ium chloride

There total 4 articles about (4S,5S)-2-((4S,5S)-1,3-bis(3,5-di-tert-butylbenzyl)-4,5-diphenylimidazolidin-2-ylideneamino)-1,3-dimethyl-4,5-diphenyl-4,5-dihydro-1H-imidazol-3-ium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 1397644-03-9
(4S,5S)-1-(3,4-di-tert-butylbenzyl)-3-(3,5-di-tert-butylbenzyl)-4,5-diphenylimidazolidin-2-imine hydrobromide

: 198625-67-1,851487-56-4
(4S,5S)-2-chloro-1,3-dimethyl-4,5-diphenylimidazolinium chloride

: 1397644-13-1
(4S,5S)-2-((4S,5S)-1,3-bis(3,5-di-tert-butylbenzyl)-4,5-diphenylimidazolidin-2-ylideneamino)-1,3-dimethyl-4,5-diphenyl-4,5-dihydro-1H-imidazol-3-ium chloride

Guidance literature:: With triethylamine; In acetonitrile; at 80 ℃; for 12h; Reflux; Inert atmosphere;
DOI:10.1021/ol302030v

Reference yield:

: 62938-08-3
3,5-di-tert-butylbenzyl bromide

: 1397644-13-1
(4S,5S)-2-((4S,5S)-1,3-bis(3,5-di-tert-butylbenzyl)-4,5-diphenylimidazolidin-2-ylideneamino)-1,3-dimethyl-4,5-diphenyl-4,5-dihydro-1H-imidazol-3-ium chloride

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate; tetrabutylammomium bromide / acetonitrile / 24 h / 20 °C

2: acetonitrile / 6 h / 80 °C / Inert atmosphere

3: triethylamine / acetonitrile / 12 h / 80 °C / Reflux; Inert atmosphere

With tetrabutylammomium bromide; potassium carbonate; triethylamine; In acetonitrile;
DOI:10.1021/ol302030v

Reference yield:

: 1397643-99-0
(1S,2S)-N¹,N²-bis(3,5-di-tert-butylbenzyl)-1,2-diphenylethane-1,2-diamine

: 1397644-13-1
(4S,5S)-2-((4S,5S)-1,3-bis(3,5-di-tert-butylbenzyl)-4,5-diphenylimidazolidin-2-ylideneamino)-1,3-dimethyl-4,5-diphenyl-4,5-dihydro-1H-imidazol-3-ium chloride

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile / 6 h / 80 °C / Inert atmosphere

2: triethylamine / acetonitrile / 12 h / 80 °C / Reflux; Inert atmosphere

With triethylamine; In acetonitrile;
DOI:10.1021/ol302030v