1,2-diphenyl-nitrobutane

Base Information

• Chemical Name: 1,2-diphenyl-nitrobutane
• CAS No.: 936854-02-3
• Molecular Formula: C₁₆H₁₇NO₂
• Molecular Weight: 255.316

Synonyms:1,2-diphenyl-nitrobutane

Chemical Property of 1,2-diphenyl-nitrobutane

Chemical Property:

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Technology Process of 1,2-diphenyl-nitrobutane

There total 1 articles about 1,2-diphenyl-nitrobutane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

(E)-(1-nitroethene-1,2-diyl)dibenzene (1215-07-2) + triethylaluminum (97-93-8) → 1,2-diphenyl-nitrobutane (936854-02-3)

Guidance literature:

With copper(I) thiophene-2-carboxylate; In diethyl ether; toluene; at -78 ℃; for 48h;

DOI:10.1002/anie.200604263

Reference yield: 89.0%

1,2-diphenyl-nitrobutane (936854-02-3) → 1,2-diphenylbutane (5223-59-6)

Guidance literature:

With hydrogen; palladium dihydroxide; In methanol; at 70 ℃; under 750.075 Torr;

DOI:10.1002/anie.200604263

Reference yield: 89.0%

1,2-diphenyl-nitrobutane (936854-02-3) → 1,2-diphenylbutylamine (127529-52-6)

Guidance literature:

With hydrogen; Rh on carbon; under 750.075 Torr;

DOI:10.1002/anie.200604263

upstream raw materials:

(E)-(1-nitroethene-1,2-diyl)dibenzene

triethylaluminum

Downstream raw materials:

1,2-diphenylbutane

1,2-diphenylbutylamine

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