(5-(mercaptomethyl)-1,3-phenylene)dimethanol

Base Information

• Chemical Name: (5-(mercaptomethyl)-1,3-phenylene)dimethanol
• CAS No.: 1246655-08-2
• Molecular Formula: C₉H₁₂O₂S
• Molecular Weight: 184.259

Synonyms:(5-(mercaptomethyl)-1,3-phenylene)dimethanol

Chemical Property of (5-(mercaptomethyl)-1,3-phenylene)dimethanol

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Technology Process of (5-(mercaptomethyl)-1,3-phenylene)dimethanol

There total 1 articles about (5-(mercaptomethyl)-1,3-phenylene)dimethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

S-3,5-bis(hydroxymethyl)benzyl ethanethioate (945490-11-9) → (5-(mercaptomethyl)-1,3-phenylene)dimethanol (1246655-08-2)

Guidance literature:

With potassium carbonate; In methanol; at 20 ℃; for 1.5h; Inert atmosphere;

DOI:10.1039/c0cc02289f

Reference yield: 68.0%

(5-(mercaptomethyl)-1,3-phenylene)dimethanol (1246655-08-2) + C39H54O12 (1246655-02-6) → C66H90O18S3 (1246655-09-3)

Guidance literature:

With Dimethyl(phenyl)phosphine; In acetonitrile; at 20 ℃; for 1h; Inert atmosphere;

DOI:10.1039/c0cc02289f

Reference yield: 59.1%

2,2-dimethylthiirane (3772-13-2) + (5-(mercaptomethyl)-1,3-phenylene)dimethanol (1246655-08-2) → (5-((2-mercapto-2-methylpropylthio)methyl)-1,3-phenylene)dimethanol

Guidance literature:

With triethylamine; In methanol; at 20 ℃; for 16h; Sealed tube;

upstream raw materials:

S-3,5-bis(hydroxymethyl)benzyl ethanethioate

Downstream raw materials:

C₆₆H₉₀O₁₈S₃

C₁₈₀H₂₄₆O₄₈S₉

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