sugiol methylether

Base Information

Chemical Name:sugiol methylether
CAS No.:901-41-7
Molecular Formula:C₂₁H₃₀O₂
Molecular Weight:314.468
Hs Code.:

Synonyms:sugiol methylether

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Chemical Property of sugiol methylether

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Technology Process of sugiol methylether

There total 1 articles about sugiol methylether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4698-08-2
(E)-geranic acid

: 901-41-7
sugiol methylether

Guidance literature:: Multi-step reaction with 12 steps

1.1: H₃PO₄ / toluene / 2 h / 100 °C

1.2: (-)-α-methylbenzylamine

2.1: 90 percent / K₂CO₃ / acetone / 3 h / 20 °C

3.1: 90 percent / LiAlH₄ / diethyl ether / 1 h / -10 °C

4.1: 75 percent / 4A molecular sieves; NaOAc; PCC / CH₂Cl₂ / 1 h / -10 °C

5.1: n-BuLi / hexane / 1 h / 20 °C

5.2: 60 percent / hexane / 4 h

6.1: 95 percent / H₂ / 10 percent Pd/C / ethanol / 20 °C

7.1: 85 percent / BF₃*Et₂O / CH₂Cl₂

8.1: 95 percent / AlCl₃ / CH₂Cl₂ / -5 °C

9.1: 95 percent / THF / 4 h / 0 °C

10.1: 90 percent / p-toluenesulfonic acid / benzene / 0.5 h / Heating

11.1: 95 percent / H₂ / 5 percent Pd/C / ethanol / 20 °C

12.1: 90 percent / CrO₃; AcOH / 0.5 h / 20 °C

With tetrahydrofuran; chromium(VI) oxide; lithium aluminium tetrahydride; n-butyllithium; aluminium trichloride; phosphoric acid; 4 A molecular sieve; boron trifluoride diethyl etherate; hydrogen; sodium acetate; potassium carbonate; toluene-4-sulfonic acid; acetic acid; pyridinium chlorochromate; palladium on activated charcoal; In diethyl ether; ethanol; hexane; dichloromethane; acetone; toluene; benzene; 1.1: Cyclization / 1.2: racemate resolution / 2.1: Methylation / 3.1: Reduction / 4.1: Oxidation / 5.1: Metallation / 5.2: Condensation / 6.1: Catalytic hydrogenation / 7.1: Cyclization / 8.1: Acetylation / 9.1: Addition / 10.1: Dehydration / 11.1: Catalytic hydrogenation / 12.1: Oxidation;