C₃₅H₃₇NO₇

Base Information

Chemical Name:C₃₅H₃₇NO₇
CAS No.:1267651-98-8
Molecular Formula:C₃₅H₃₇NO₇
Molecular Weight:583.681
Hs Code.:

C<sub>35</sub>H<sub>37</sub>NO<sub>7</sub>

Synonyms:C₃₅H₃₇NO₇

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Chemical Property of C₃₅H₃₇NO₇

Chemical Property:

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Technology Process of C₃₅H₃₇NO₇

There total 20 articles about C₃₅H₃₇NO₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: C₃₅H₃₅NO₇

: 1267651-98-8
C₃₅H₃₇NO₇

: 1267652-12-9
C₃₅H₃₇NO₇

Guidance literature:: With sodium tetrahydroborate; In methanol; at -78 ℃; for 2h; optical yield given as %de; Inert atmosphere;
DOI:10.1021/ol103094j

Reference yield:

: 1267651-79-5
C₃₀H₄₅NO₆Si

: 1267651-98-8
C₃₅H₃₇NO₇

Guidance literature:: Multi-step reaction with 13 steps

1.1: tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine / 1,2-dichloro-ethane / 12 h / 50 °C / Inert atmosphere

2.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

3.1: toluene-4-sulfonic acid / methanol / 2 h / 20 °C

4.1: Dess-Martin periodane / dichloromethane / 1 h / 20 °C

5.1: tetrahydrofuran / 0 - 20 °C / Inert atmosphere

6.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere

6.2: 0 - 20 °C / Inert atmosphere

7.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

8.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 2 h / 50 °C / Inert atmosphere

9.1: propan-1-ol; potassium hydroxide / water / 12 h / Reflux

10.1: sodium carbonate / tetrahydrofuran; water / 3 h / 0 °C

11.1: oxone; Na₂EDTA; 1,1,1-trifluoro-2-propanone; sodium hydrogencarbonate / water; acetonitrile / 3 h / 0 °C

12.1: Dess-Martin periodane / dichloromethane / 20 °C

13.1: tetrahydrofuran / -78 - 0 °C / Inert atmosphere

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; propan-1-ol; oxone; 1,1,1-trifluoro-2-propanone; Na₂EDTA; tetrabutyl ammonium fluoride; sodium hexamethyldisilazane; tetra-(n-butyl)ammonium iodide; sodium hydrogencarbonate; sodium carbonate; Dess-Martin periodane; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; potassium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; 1,2-dichloro-ethane; acetonitrile; 13.1: Grignard reaction;
DOI:10.1021/ol103094j

Reference yield:

: 1267651-86-4
C₃₂H₃₉NO₅Si

: 1267651-98-8
C₃₅H₃₇NO₇

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere

1.2: 0 - 20 °C / Inert atmosphere

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

3.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 2 h / 50 °C / Inert atmosphere

4.1: propan-1-ol; potassium hydroxide / water / 12 h / Reflux

5.1: sodium carbonate / tetrahydrofuran; water / 3 h / 0 °C

6.1: oxone; Na₂EDTA; 1,1,1-trifluoro-2-propanone; sodium hydrogencarbonate / water; acetonitrile / 3 h / 0 °C

7.1: Dess-Martin periodane / dichloromethane / 20 °C

8.1: tetrahydrofuran / -78 - 0 °C / Inert atmosphere

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; propan-1-ol; oxone; 1,1,1-trifluoro-2-propanone; Na₂EDTA; tetrabutyl ammonium fluoride; sodium hexamethyldisilazane; sodium hydrogencarbonate; sodium carbonate; Dess-Martin periodane; potassium hydroxide; In tetrahydrofuran; dichloromethane; water; acetonitrile; 8.1: Grignard reaction;
DOI:10.1021/ol103094j