4-(m-toluidino)-6-(3-aminopropoxy)-2-(ethylamino)pyrimidine-5-carboxamide.

Base Information

Chemical Name:4-(m-toluidino)-6-(3-aminopropoxy)-2-(ethylamino)pyrimidine-5-carboxamide.
CAS No.:1374158-77-6
Molecular Formula:C₁₇H₂₄N₆O₂
Molecular Weight:344.417
Hs Code.:

Synonyms:4-(m-toluidino)-6-(3-aminopropoxy)-2-(ethylamino)pyrimidine-5-carboxamide.

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Chemical Property of 4-(m-toluidino)-6-(3-aminopropoxy)-2-(ethylamino)pyrimidine-5-carboxamide.

Chemical Property:

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Technology Process of 4-(m-toluidino)-6-(3-aminopropoxy)-2-(ethylamino)pyrimidine-5-carboxamide.

There total 8 articles about 4-(m-toluidino)-6-(3-aminopropoxy)-2-(ethylamino)pyrimidine-5-carboxamide. which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1374160-08-3
C₂₂H₃₂N₆O₄

: 1374158-77-6
4-(m-toluidino)-6-(3-aminopropoxy)-2-(ethylamino)pyrimidine-5-carboxamide.

Guidance literature:: With trifluoroacetic acid; In dichloromethane;

Reference yield:

: 868272-41-7
2-(ethylthio)-4-(methylthio)-6-oxo-1,6-dihydropyrimidine-5-carbonitrile

: 1374158-77-6
4-(m-toluidino)-6-(3-aminopropoxy)-2-(ethylamino)pyrimidine-5-carboxamide.

Guidance literature:: Multi-step reaction with 8 steps

1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 48 h / 45 °C

2: sulfuric acid / trifluoroacetic acid / 2 h / 85 °C

3: butan-1-ol / 0.33 h / 0 - 20 °C

4: 3-chloro-benzenecarboperoxoic acid / 1-Methylpyrrolidine; tetrahydrofuran / 8 h / 0 °C

5: N-ethyl-N,N-diisopropylamine / 1-Methylpyrrolidine; tetrahydrofuran / 20 °C

6: 3-chloro-benzenecarboperoxoic acid / 1-Methylpyrrolidine / 3 h / 20 °C

7: 1-Methylpyrrolidine; tetrahydrofuran / 20 °C

8: trifluoroacetic acid / dichloromethane

With sulfuric acid; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; trifluoroacetic acid; In tetrahydrofuran; 1-Methylpyrrolidine; dichloromethane; N,N-dimethyl-formamide; butan-1-ol;

Reference yield:

: 1374158-79-8
tert-butyl 3-(5-cyano-2-(ethylthio)-6-(methylthio)pyrimidin-4-yloxy)propylcarbamate.

: 1374158-77-6
4-(m-toluidino)-6-(3-aminopropoxy)-2-(ethylamino)pyrimidine-5-carboxamide.

Guidance literature:: Multi-step reaction with 7 steps

1: sulfuric acid / trifluoroacetic acid / 2 h / 85 °C

2: butan-1-ol / 0.33 h / 0 - 20 °C

3: 3-chloro-benzenecarboperoxoic acid / 1-Methylpyrrolidine; tetrahydrofuran / 8 h / 0 °C

4: N-ethyl-N,N-diisopropylamine / 1-Methylpyrrolidine; tetrahydrofuran / 20 °C

5: 3-chloro-benzenecarboperoxoic acid / 1-Methylpyrrolidine / 3 h / 20 °C

6: 1-Methylpyrrolidine; tetrahydrofuran / 20 °C

7: trifluoroacetic acid / dichloromethane

With sulfuric acid; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; trifluoroacetic acid; In tetrahydrofuran; 1-Methylpyrrolidine; dichloromethane; butan-1-ol;