allyl 2-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-3-O-carbamoyl-4-O-(3-(trifluoromethyl)-benzoyl)-α-D-galactopyranosiduronamide

Base Information

Chemical Name:allyl 2-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-3-O-carbamoyl-4-O-(3-(trifluoromethyl)-benzoyl)-α-D-galactopyranosiduronamide
CAS No.:220974-57-2
Molecular Formula:C₃₂H₃₈F₃N₃O₁₆
Molecular Weight:777.659
Hs Code.:

allyl 2-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-3-O-carbamoyl-4-O-(3-(trifluoromethyl)-benzoyl)-α-D-galactopyranosiduronamide

Synonyms:allyl 2-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-3-O-carbamoyl-4-O-(3-(trifluoromethyl)-benzoyl)-α-D-galactopyranosiduronamide

Suppliers and Price of allyl 2-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-3-O-carbamoyl-4-O-(3-(trifluoromethyl)-benzoyl)-α-D-galactopyranosiduronamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of allyl 2-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-3-O-carbamoyl-4-O-(3-(trifluoromethyl)-benzoyl)-α-D-galactopyranosiduronamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of allyl 2-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-3-O-carbamoyl-4-O-(3-(trifluoromethyl)-benzoyl)-α-D-galactopyranosiduronamide

There total 4 articles about allyl 2-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-3-O-carbamoyl-4-O-(3-(trifluoromethyl)-benzoyl)-α-D-galactopyranosiduronamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 2251-65-2
3-(Trifluoromethyl)benzoyl chloride

: 148944-30-3
allyl 2-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-3-O-carbamoyl-α-D-galactopyranosiduronamide

: 220974-57-2
allyl 2-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-3-O-carbamoyl-4-O-(3-(trifluoromethyl)-benzoyl)-α-D-galactopyranosiduronamide

Guidance literature:: With pyridine; dmap; at 20 ℃; for 1.5h;
DOI:10.1016/S0040-4020(98)01225-3

Reference yield: 28.0%

: 2251-65-2
3-(Trifluoromethyl)benzoyl chloride

: 148944-30-3
allyl 2-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-3-O-carbamoyl-α-D-galactopyranosiduronamide

: allyl 2-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-3-O-carbamoyl-4-O-(3-(trifluoromethyl)-benzoyl)-α-D-galactopyranosidurononitrile

: 220974-57-2
allyl 2-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-3-O-carbamoyl-4-O-(3-(trifluoromethyl)-benzoyl)-α-D-galactopyranosiduronamide

Guidance literature:: With pyridine; at 20 ℃; for 3.5h;
DOI:10.1016/S0040-4020(98)01225-3

Reference yield:

: 148944-29-0
allyl 2-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-α-D-galactopyranosiduronamide

: 220974-57-2
allyl 2-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-3-O-carbamoyl-4-O-(3-(trifluoromethyl)-benzoyl)-α-D-galactopyranosiduronamide

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) bis(tri-butyltin) oxide / 1.) CHCl₃, 1 h, reflux, 2.) CHCl₃, 0 deg C, 1 h

2: Zn / methanol / 20 °C

3: 64 percent / pyridine / 3.5 h / 20 °C

With pyridine; bis(tri-n-butyltin)oxide; zinc; In methanol;
DOI:10.1016/S0040-4020(98)01225-3